GCMS data file header for May 24-28, 2002

NYC 9/11 Public Portal Document Llprary searcn compound Report

Data File : C:\MSDCHEM\l\DATA\052802\524LB.D Vial: 3 Acq On : 28 May 2002 3:56 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan ** Library : C:\DATABASE\NIST98.L

Peak Number 9 Phenanthrene, 9-methyl- Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

22.54 0.25 ug/L 244677 Phenanthranerie-dlO • 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 ~~ 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 45 S 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 40 — 4 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 40 Abundance Scan 3312 (22.539 min): 524LB.D (-3296) (-) m/z 192.10 100.00% 192

5000

— ro 96 146 160 22.20 22.40 22.60 22.80 44 52 70 82 j 118 I 1 0- < | | ‘ । | । 'I I| I I > I | I > 1> | 1 1 I q1 > 1 I| >II 1|I II I| II II|I!I I( 1 1 1 1 | I 1 | ! 1 1I III I > | ■ 1 II| m/z 191.00 20.89% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 19/2

5000 22.20 22.40 22.60 22.80 m/z 193.00 14.76% _ 96 165 , , 29 39 51। 01 , (.’I 63 74 . 11'. 83 . 11. JI'I 11.,,, । 115, 111126 139 152 ,| 176 , > 1111 rl'| 11111'11111 i'1'i 111 ili ।, i i’rtT-r|-n niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 164 22.20 22.40 22.60 22.80 5000 99 m/z 146.00 12.57% 115 47 67 77 177 146 01+27.3844574 27 3ft 125134 -7-+— 4155, nodhponn 4-— 133 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125844: Anthracene, 2-methyl- _A 192 22.20 22.40 22.60 22.80 m/z 95.90 11.45% 5000

nfe-> 0: .............................. ... 93 96 ......... 115 139 150 ,1 176 165 ■ i “ ■' t ■ ■" । ■' ■ ■ । •11" m "1 r1111111111111 11 rn 11111! 11 > i i'i 11 ii]-! i rTrt ■ 11 > I > TTi’ 20 30 40 50 60 70 80 90 100 110120130 140 150 160 170 180 190 200 u 22.20 22.40 22.60 22.80

524LB.D 052202.M Thu May 30 10:44:17 2002 Page 12

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