GCMS quantitation report, sample LB, June 2002

NYC 9/11 Public Portal Document Library searen compound Report Data File : C:\MSDCHEM\l\DATA\061102\LB.D Vial: 4 Acq On : 11 Jun 2002 12:19 pm Operator: Sample : gc/ms scan 6/11 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 19 Phenanthrene, 9-methyl- Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.25 ug/L 279418 Phenanthranene- dl 0 22.91 Hit# of Tentative ID MW MolForm CAS# Qual 1 Phenanthrene , 9-methyl- 192 C15H12 000883-20-5 59 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 59 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 59 Abundance ′ Scan 3311 (22.533 min): LB.D (-3305) (-) m/z 192.00 100.00% 192

5000

40 54 70 82 %6 120 146 160 .... n..... 22.20 22.40 22.60 22.80 0 . I .... 1 .... I I I l rI /1 I | I I I I | | | | | | Ht ; I I I | | | n-f 1 tHpmp - m/z 146.10 17.21% mfz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl-. 192

5000 1 22.20 22.40 22.60 22.80 m/z 191.00 16.34% 29 39 51 63 74 83 * 115 126 139 152 165 176 1 0 TPWTTTTTOTITTTTTTTTRTTTTTTTTTTTHmT ■■ i" n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125844: Anthracene, 2-methyl- 192

22.20 22.40 22.60 22.80 5000 m/z 193.10 15.96%

63 96 165 63 74 T. ll 115 139 150 1 176 . 0 ‘ I ‘ “ I “ “ I " • ' I " ' ‘ I ‘ ' l ‘ f“ I4'' i’ri l H > | . 1 . l p I'l . | > . 1 1 | 1 1 I l’| . . . . 1 1 1 mn Tilipuni mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl- TTI 192 22.20 22.40 22.60 22.80 m/ z 96.00 11.86%

5000

_ 96 165 28 39 51 63 74 83 1 105 115 126 139 152 1 176 0 11 । i rtp i i ,‘|-i i ■. |’i 11. [ r’M i| i ITi frtlrrl i-| i i ।. 11 i 11 MTrn i |'I i i i Tll 111 rt 1111 r II’T m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

LB.D 060302.M Tue Jun 11 15:55:51 2002 Page 22

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