GCMS quantitation report, sample LB, June 2002

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Data File : C:\MSDCHEM\1\DATA\061102\LB.D Vial: 4 Acq On : 11 Jun 2002 12:19 pm Operator: Sample : gc/ms scan 6/11 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 20 Anthracene-dlO- Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.31 ug/L 341210 Phenanthranene -dl 0 22.91 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-d10-// 188 C14D10 001719-06-8(90 2 3-Amino/4-methylx6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 3 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 40 4 Pentac^clo[7.3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 39 Abundance Scan 3401 (23.062 min): LB.D (-3393) (-) • m/z 188.10 100.00% 188

5000

80 94 158 22.80 23.00 23.20 23.40 0- ‘.............. 40 51 66| I i “ " i “ “ i ■ “11 “ “ i ■ ■ ■ • i “111 “11 “ “ 11 ' ITT mm ‘I “ “ i m/z 94.05 16.51% miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

/ 5000 ' ' i ■ ■ ' • i • 22.80 23.00 23.20 23.40 m/z 189.20 13.72% 80 94 160 . । 17 30 42 52 66 108118 132 146 11 170179.,! 0 | | I I I I | I I I I | I I ! mH | ' n " " i1 ■" i1 TIHNTN11 miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188

145 22.80 23.00 23.20 23.40 5000 m/z 80.05 12.46%

117

n/z-> 0 ----- 41 51 63 77 89 102 130

10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 -mm 159 173 I I Abundance #1 25696:2-Quinolinecarboxaldehyde, 8-hydroxy- oxime 188 22,80 23.00 23,20 23.40 m/z 184.00 12.12% 5000 143 89 115 51 64 64 76 T 102 I, 130 | 158 170 | 0- ‘ i “ " 111' ■ i.'" ■ i" ■' I'1 •11 pl ■ " ’ll 11 ■ II . i.. 11 r.. । < I 1111 ilr 11 ( 111111 pi 1111'1111111 II 11111 m/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

LB.D 060302.M Tue Jun 11 15:55:55 2002 Page 23

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