GCMS sample AE12743 results, June 10 2002

NYC 9/11 Public Portal Document ubrary searcn compound Keporc Data File C:\MSDCHEM\l\DATA\060602\12761.D Vial: 7 Acq On 6 Jun 2002 4:11 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 20 Anthracene-dlO- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.30 ug/L 300343 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 87 2 Phenanthrene-diO 188 C14D10 001517-22-2 47* 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 37 Abundance Scan 3401 (23.062 min): 12761 .D (-3394) (-) m/z 188.10 100.00 188

5000

80 94 TTT 42 52 66 160 22.80 23.00 23.20 23.40 0 TTTWTTTTTTTHTTTHTT- m/z 94.20 19.23% /z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 118

5000 1 1 i 1 1 i 1 22.80 23.00 23.20 23.40 m/z 184.00 16.58% 17 30 42 52 0 160 108118 132 146 |L 0 TIUTTTTTTTHTTmmmmmt | 170179) 80 , ,94 TT iz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/ z 80.05 15.48%

94 • 80 160 30 42 52 11 108118 66 132 146 1. 170179,,! TTTmm 0 T|i ■ i < । > > TI > i I I | I | I I | tTTi I I | I | I'l T TT m/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 1 188 22.80 23.00 23.20 23.40 m/z 189.10 12.72% 145 5000

117 41 51 63 77 89 102 130 I 159 173 1 m/z—> 0 --------------- 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 II 22.80 23.00 23.20 23.40

12761.D 060302.M Mon Jun 10 10:25:34 2002 Page 23

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