GCMS analysis results for sample AE11152, May 2002

NYC 9/11 Public Portal Document uDaty searcn compound Keporc Data File : C:\MSDCHEM\1\DATA\020515\11152 .D Vial: 18 Acq On : 16 May 2002 4:35 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.37 ug/1 41602 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-d10 188 C14D10 001517-22-2 50 3 Ancipyrine 188 C11H12N2O 000060-80-0 49 4 Antipyrine 188 C11H12N2O 000060-80-0 47 Abundance Scan 4916 (31.963 min): 11152.D (-4907) (-) m/z 188.15 100.00% 168

5000

66 80 94 158 31.60 31.80 32.00 32.20 ...... nz->_______ 20 —4 4+96111 40 60 1177 80 11 100 0 .... 120 2000011110 140 160 180 204 217 200 220 rn/z 94.20 13.99% Abundance #79826: Anthracene-d 10- 188

5000 "I 1TI 1 1 ‘"[ i > > j -I 31.60 31.80 32.00 32.20 m/ z 80.00 13.47% 80 94 .160 , , 17 30 42 52 66 —l 108118 132 146.-1179 ll. mZz->_______ 20 1 77 t-/. i I'. Ui 40 60 1 80 100 120 140 160 180 200 i 1 ' ■ ■ i ' 220 Abundance #79827: Phenanthrene-d10 1(18 / 31.60 31.80 32.00 32.20 5000 m/z 189.05 13.34%

80 94 160 30 42 52 66 . , । । । . 77 । । ~ । l ■ ■ । ■ 111 । 111 ■) 108118. 132 146 + 170 )........ m/z-> 20 40 60 80i 100 120 140 160 180 200 220 Abundance #125688: Antipyrine I ' ' ‘ ■ i ■ ■ ■ ■ i 1 188 31.60 31.80 32.00 32.20 96 m/z 158.00 12.12% 5000 77 56

— 39 106 I 67 liii. .1 .1 — 141 1 1 i 1 1 1 ■ I * ■ 1 1 , 1111116129 145 'I 1 1 11 1 . I 1 11 1 । 159 173 ll . n/z—> 20 40 60 80 100 120 140 160 180 200 220 31.60 31.80 32.00 32.20

11152.D SCAN020507.M Thu May 16 09:28:38 2002 Page 7

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