GCMS analysis results, sample AE12288, June 2002

NYC 9/11 Public Portal Document ulDrary searcn compound KeporL

Data File : C:\MSDCHEM\1\DATA\052902\12288.D Vial: 7 Acq On : 29 May 2002 2:58 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 15 Anthracene-diO- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.30 ug/L 316041 Phenanthranerie-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 74 2 Antipyrine 188 C11H12N2O 000060-80-0 40 3 Antipyrine 188 C11H12N2O 000060-80-0 40 4 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 40 Abundance Scan 3402 (23.068 min): 12288.D (-3394) (-) m/z 188.10/100.00% 188

5000

80 94 - 66 158 22.80 23.00 23.20 23.40 44 0- .......................... ‘ ' 1 pail ----mmmHH—p-rrr m/z 94.00 21.71% m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 80.10 17.68% 42 52 66 7 94 _ 160 , . 17 30 108118 132 146 I 170179|.i | 0- ■ 1111 n 1111 > । rl-111 n 11 j 11 n | TI—*]eammhH—Hmm*mau niz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #125690: Antipyrine 188

96 22.80 23.00 23.20 23.40 5000 77 m/z 189.05 15.21% 56 105 43 , I 67 rhmtmmmmm1U 115 129 159 173 > 0 n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79725: Antipyrine 188 22.80 23.00 23.20 23.40 96 m/z 184.10 13.67%

5000 77 56 105 27 39 59 67 । , || 115 130 145 159 173 n/z-> 0 TT’t --+++ > ’t । rPh pi illl-p’i । i ’r r । rt । n i 111Jh 11111' 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 JU - 22.80 23.00 23.20 23.40

12288.D 052202.M Mon Jun 03 09:37:15 2002 Page 18

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