GCMS analysis results, sample AE12288, June 2002

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Data File : C:\MSDCHEM\l\DATA\052902\12288.D Vial: 7 Acq On : 29 May 2002 2:58 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Thiacyclohexane-3-ol Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

34.81 0.48 ug/L 181720 Perylene-d12 34.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Thiacyclohexane-3-ol 118 C5H10OS 1000145-72-1 7 2 trans-2-Ethoxy-b-methyl-b-nitros... 207 C11H13NO3 134040-21-4 5 3 1,2-Naphthalenediol, 2-ethyl-l,2... 206 C13H1802 056588-34-2 4 4 Naphthalene, 1,2,3,4-tetrahydro-... 146 C11H14 001680-51-9 4 Abundance Scan 5400 (34.807 min): 12288.D (-5399) (-) m/z 118.00 100.00% 118 131

256 5000 207 49 34.40 34.60 34.80 35.00 35.20 0!TIT m/z 131.30 94.00% miz-> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #52739: Thiacyclohexane-3-ol 61 1 8 43

5000 74 — 1 1 ' ‘ ■ i ■ AA-A--— 85 34.40 34.60 34.80 35.00 35.20 | 100 m/z 256.00 60.00% 0 i■ ■■ ■i 1 , ILLIH ‘ i 1 ■ 1 ■ i ‘ ' i ■ 1 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #59317: trans-2-Ethoxy-b-methyl-b-nitrostyrene 131 - .8 . n , . 34.40 34.60 34.80 35.00 35.20 5000 m/z 262.10 57.20% 77 105 207 43 91 145 160 1 I 65 1 0- ........ II 77 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #52959:1,2-Naphthalenediol, 2-ethy-1,2,3,4-tetrahydro-1-... ■ i ■ ■ ‘ ■ i 1 ■ 1- 8 34.40 34.60 34.80 35.00 35.20 131 m/z 207.00 44.80% 159 5000 91 57 29 188 206 43 77 106 ll 145

miz—> 0 —4 20 40 +44—4+ 60 i., 1ll, lll +4 80 100 120 140 160 180 200 220 240 260 173 — the , i f . i ।u i i i । . i . । . r 34.40 34.60 34.80 35.00 35.20

12288.D 052202.M Mon Jun 03 09:37:16 2002 Page 19

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