GCMS analysis results for sample AE11152, May 2002

NYC 9/11 Public Portal Document LLprary bedrcr compound Keporc

Data File : C:\MSDCHEM\l\DATA\020515\11152.D Vial: 18 Acq On : 16 May 2002 4:35 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Bitoscanate Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.08 0.32 ug/1 36789 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Bitoscanate 192 C8H4N2S2 004044-65-9 58 2 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 50 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 50 4 3-(^-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 45 Abundance Scan 4766 (31.082 min): 11152.D (-4758) (-) m/z 192.20 100.00% 192

5000 ,.A "AA A-4, I I I 44 82 30.80 31.00 31.20 31.40 . , |IL , shoa 120,) .'i160 I ■ ■ ............................................................. 444 m/ z 82.00 15.67% m/z—> 50 100 150 200 250 300 350 400 450 Abundance #125828: Bitoscanate 192

5000 ■ ■ i ■ ■ ■ ‘ i ■ 30.80 31.00 31.20 31.40 134 m/z 193.10 15.34% 90 160

mlz—> 44414 50 100 150 200 250 300 350 400 450 Abundance #125856: Phenanthrene, 1-methyl- 192 ............... ........................ 30.80 31.00 31.20 31.40 5000 m/ Z 44.00 14.66%

96 1RR 39 63.1 116 139 117, _ ' I ‘ ' r ■ i ■ ■ ■ ■ r ■ ‘ “ 1 I ' ‘ * V m/z-> 50 100 150 200 250 300 350 400 450 Abundance #81033: Phenanthrene, 9-methyl- ■ 'i' i 1 ■ ' ' i ■ 1 192 30.80 31.00 31.20 31.40 m/z 49.10 14.25%

5000

96 165 | A 39 63 TTu A 116139,1, 4, /z—> 50 100 150 200 250 300 350 400 450 30.80 31.00 31.20 31.40

11152.D SCAN020507.M Thu May 16 09:28:38 2002 Page 6

NYC-WTC_000024481