Gas chromatography-mass spectrometry analysis of sample AE10987 completed May 22, 2002, showing unknown compounds and surrogate recovery at 89%.
NYC-WTC_000024463–000024471Folder label: “GCMS X 5/13/02 A 5/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Llprary searcn compound Keporc
Data File : C:\MSDCHEM\1\DATA\020515\10987.D Vial: 17 Acq On : 16 May 2002 3:36 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2
R.T. EstConc Area Relative to ISTE R.T.
31.96 0.28 ug/1 31584 Phenanthrene-dl0 31.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1—PheildiiLhrene-dl 0 188 C14D10 001517-22-2 81 2 Anthracene-dlO- 188 C14D10 001719-06-8 74 3 Antipyrine 188 C11H12N2O 000060-80-0 47 4 Antipyrine 188 C11H12N2O 000060-80-0 43 Abundance Scan 4915 (31.958 min): 10987.D (-4907) (-) m/z 188.15 100.00% 188
5000 80 52 158 31.60 31.80 32.00 32.20
mfe-> 11,94/112.. "I""i '''I'I i1' 321 ■ 1 । 1 1 1 1 । ■ ■ 1 ■ । 1 " 1 । 1 1 1 1 i 1 1 1 1 i 1 1 1 1 i' 1 1 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 m/z 79.90 32.64%
Abundance #79827: Phenanthrene-d10 188
5000 M 31.60 31.80 32.00 32.20 m/z 158.20 17.17% 80 94 160 28 42 66 j —pp —mmmJ il 108 132 '1111''1111111111111111111' mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #79826: Anthracene-d10- 188
31.60 31.80 32.00 32.20 5000 m/z 184.20 16.97%
80 94 160 28 42 .66 11I1111 ’ 1‛1‛t—L —l "'I 118132 ,|| 'I''"'1]'" ■ > i ■ ■ ■' i ■ ■ ■ ■ i ■ ■ •' i ■ ■'11 ■'1 ■ i ‘ ■ i1 ■ iz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #79725: Antipyrine 188 31.60 31.80 32.00 32.20 96 m/z 189.00 16.78% 5000 77 56 39 . 115130144159173 . TTTTTT rhh iU 11 101 111111111 tTTr1 '1'1 " I' 1’1-11111111111111111113—311"7"7-T II’* TTr i r-r । । i-1 r । . i i । । । m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 31.60 31.80 32.00 32.20
10987.D SCAN020507.M Thu May 16 09:24:44 2002 Page 4
NYC-WTC_000024470
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NYC-WTC_000024565
Laboratory report documenting GCMS analysis of sample AE11283 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022588
Laboratory report of GCMS analysis for sample AE11482 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024575
Laboratory report documenting GCMS analysis of sample AE11285 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024770
Laboratory report of GCMS analysis for sample AE10241 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024681
Laboratory report documenting GCMS analysis of sample AE11159 conducted on May 22, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024719
Laboratory report documenting GCMS analysis of sample AE11279 conducted on May 22, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024613
Laboratory report documenting GCMS analysis of sample AE11305 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024380
Chain of custody record for GCMS analysis of sample AE10237 on May 20, 2002, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024472
Laboratory report documenting GCMS analysis of sample AE11152 conducted on May 22, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024484
Laboratory report documenting GCMS analysis of sample AE11153 conducted on May 22, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022598
Laboratory report of GCMS analysis for sample AE11566 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046138
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10068 on May 17, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000024423
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000024424
Brief log entry or header page from a GCMS analysis record dated between May 13 and May 16, 2002.
Filed in the same folder
NYC-WTC_000024427
Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.
Filed in the same folder
NYC-WTC_000024437
Laboratory report showing calibration results for volatile organic compounds using GCMS methods between May 13 and May 15, 2002.
Filed in the same folder
NYC-WTC_000024441
Laboratory record of reference standard analysis for volatile organic compounds using GCMS methods from May 13 to May 15, 2002.
Filed in the same folder