GCMS analysis report sample AE09519, May 23, 2002

NYC 9/11 Public Portal Document LLDrary searcn compound Keporc

Data File : C:\MSDCHEM\1\DATA\052102\9519.D Vial: 14 Acq On : 21 May 2002 11:55 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 Phenanthrene-diO Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.24 ug/L 216049 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 00 1 5 1 7 - 22 - 2 80) 2 Anthracene-dlO- 188 C14D10 001719-06-8 64” 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 4 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 40 Abundance Scan 3402 (23.068 min): 9519.D (-3396) (-) m/z 188.10 100.00% 1(8

5000

80 94 42 52 66 i 0 IWPITPIWITTTHITOTTTT 132 m 160 22.80 23.00 23.20 23.40 m/z 189.10 15.90 ‘I miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance Phenanthrene-d10 1(8

5000 22.80 23.00 23.20 23.40 m/z 94.10 15.77%| 80 94 160 30 42 52 66 , ,l| 108118 132 146 I. 170179.1,1 I 0 TI—B—mmmp—am——ua—napt 1 11'1 1111 j H • i th ri [ i'i i j 7 11 rrtrt rr 11!: j i rl'l |‘i j i rt 11 111'11111 j 111 J' miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1(8 — 22.80 23.00 23.20 23.40 5000 m/z 80.10 14.31

RR 80 94 160 17 30 42 52 68 ,| 108118 132 146 II 170179|,i 0 PTHt 1111111111111 ii 11 [ 11 n 111 i’i । n fl’t [. । [ । ii i [MMI Wt nfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoIine 1(8 22.80 23.00 23.20 23.40 m/z 184.10 12.99 145 5000

117 159

n/z—> 0- 41 51 63 77 89 102

10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 130 173 Hl—nr i"1 I I 22.80 23.00 23.20 23.40

9519.D 052202.M Wed May 22 11:32:46 2002 Page 14

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