GCMS sample AE12764 results, June 10 2002

NYC 9/11 Public Portal Document Llorary searcn compound Keport

Data File C:\MSDCHEM\l\DATA\060702\12764.D Vial: 4 Acq On 7 Jun 2002 11:02 am Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 19 Phenanthrene-diO Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.27 ug/L 244987 Phenant hr anene - dl 0 22.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 80 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 36 Abundance Scan 3401 (23.062 min): 12764.D (-3392) (-) m/z 188.10 100.00% 188

5000

40 51 . 80 94 160 Ju l 1 * ‘ ’ I 22.80 23.00 23.20 23.40 1BT

0 TTTTTTTTTT 1’1111115231/1/11111/1110111333111 1 ■" ■ i m/ Z 94.10 18.84% iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 80 m/z 189.10 18.54% 94 160 30 42 52 66 niz-> 0 TTTTTTTPTTTTHTTHTT 11 108118 132 146 I 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 1791791.. Abundance #79826: Anthracene-d10- 118 - 22.80 23.00 23.20 23.40 5000 m/z 184.10 16.51%

80 94 160 , . 17 30 42 52 66 . —108118.132.146—4179179— 0 ' i ■ ■ ■ ■ I' ■1 ■ i ■ ■ 111111111111.| 111111111 11111 n/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 ........... .............................. Abundance #79771:3-Amino-4-methyI-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/z80.00 9.52% 145 5000

41 51 63 77 89 102 117 130

m/z—> 0 ------- I 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 J 1 22.80 23.00 23.20 23.40

12764.D 060302.M Mon Jun 10 10:30:08 2002 Page 22

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