GCMS analysis results, sample AE12479, June 2002

NYC 9/11 Public Portal Document Llprary searcn Compound Report Data File : C:\MSDCHEM\1\DATA\052902\12479.D Vial: 21 Acq On : 30 May 2002 2:22 am Operator: McLean Sample : gc/ms scan 5/28 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 15 Anthracene-dlO- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T. 23.07 0.28 ug/L 282379 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual -

1 Anthracene-dlO- 188 C14D10 001719-06-8 90- 2 Phenanthrene-diO 188 C14D10 001517-22-2 78 // 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) ... 188 C14H20 1000215-61-8 42 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 Abundance Scan 3402 (23.068 min): 12479.D (-3395) (-) m/z 188.10 100.00% 188

5000

80 94 158 22.80 23.00 23.20 23.40 0 -0,49 l 132 i ■ “ ■ i■■" ।1■ ■ ■ i ■ ■ T I‘‘3T m/ z 80.10 19.74% niz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1tl8

5000 22.80 23.00 23.20 23.40 m/z 189.10 17.57% 80 94 160 , , 17 30 42 52 66 , 108118 132 146 111.170179 ,1 0 ■ i “ “ i ■" ■ i “ THhtt —PTHmmtmon n/z-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 11®

22.80 23.00 23.20 23.40 5000 m/ z 94.10 16.04%

80 94 160 30 1142 52 66 108118 132 146 ,|.I 170179.1,1 0- 1 “111" " 11' 111111I I111 rl 11111 l l 1 1 11 [ I L r1HTTT niz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... 110 22.80 23.00 23.20 23.40 m/z 187.20 12.09% 5000 79 91 55 67 10= 117 105 131 145 159 0 ' 111'11 “ “ I'1" i11" I — mhmmmt 173 TUuI.. —TTT l - miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12479.D 052202.M Mon Jun 03 11:42:02 2002 Page 18

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