GCMS analysis results, sample AE12479, June 2002

NYC 9/11 Public Portal Document Llbrary Search compound Report Data File : C:\MSDCHEM\l\DATA\052902\12479 .D Vial: 21 Acq On : 30 May 2002 2:22 am Operator: McLean Sample : gc/ms scan 5/28 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Anthracene, 2-methyl- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.25 ug/L 253120 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 530 3 2-Propenal, 3-(3,4-dimethoxyphen.... 192 C11H1203 004497-40-9 42 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 38 Abundance Scan 3312 (22.539 min): 12479.D (-3306) (-) m/z 192.05 100.00% 192

5000 - 92 96 146 160 22.20 22.40 22.60 22.80 122 44 70 L, .I 0 h-p-TT-rp-rTTp-l-rrpT-rTpTTTfTT^^ (। > i rr | > 11, ।.... । , .'11111 ■ ■ J11111 i rTT|-, 11 । J1 Hm m/z 191.00 24.93% /z-> 20 30 40 50 60 70 80 90 100 110120 130140150 160170 180 190 200 Abundance #125845: Anthracene, 2-methyl- 192

5000 ■ ■ i 1 ■ ■ ■ । • ■ ■ ■ ।1 1 1 1 i 1 ' 1 ' i 22.20 22.40 22.60 22.80 m/z 193.00 16.33% 66 75 87 T 115 126 139 152 155 176 0 TTmmmtmmmhptppn ’ 1pn miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 152 1— 22.20 22.40 22.60 22.80 5000 m/ z 96.00 14.02%

29 39 51 63 74 83 T 115 126 139 152 165 176 J, | 0 I(I«... j J . [l’ rl 1111 > । ■ i n | rri Fpri 11111'| 111 > |-| 11 ■ p’ri ij i rH 111 i’r’tt 7’1’1 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- "IT 192 22.20 22.40 22.60 22.80 161 m/z 146.10 12.72% 5000 77 91 121 149 177 52 64 138

n/z—> 0 mmmmH 1.... 1 •11 “ ■ ■ i ‘ - tpn 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 -A 22.20 22.40 22.60 22.80

12479.D 052202.M Mon Jun 03 11:42:00 2002 Page 17

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