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GC/MS results for unknown compounds and surrogates, sample AE10980, May

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS analysis of sample AE10980 with surrogate recovery data for 2,4-DDD.

NYC-WTC_000023887–000023903

Folder label: “GCMS X 5/10/02 A 5/14/02

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NYC 9/11 Public Portal Document Llbrary Search Compound Report Data File : C:\MSDCHEM\1\DATA\051402\10980.D Vial: 9 Acq On : 14 May 2002 8:01 pm Operator: Mclean Sample : 5/10 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Phenanthrene-diO Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 23.11 0.47 ug/L 520883 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 87 2 Anthracene-diO- 188 C14D10 001719-06-8 87 3 2-Methyl-2 ,3-epoxy-2,3-dihydro-l... 188 C11H8O3 015448-59-6 47 4 Naphthalene, 2,6-dimethoxy-188 C12H1202 005486-55-5 42 Abundance Scan 3409 (23.109 min): 10980.D (-3401) (-) m/z 188.10 100.00% 188

5000

1 1 i ' ' ■ P 1 i 1 1 , 1 1 ' I 80 94 c 22.80 23.00 23.20 23.40 41 . 57 66 .11 160 0'i 11111 j ■ i ■ 11 ■ mmmmmmmmpm ——— m/z 189.10 12.65% m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 ...1.... .... 22.80 23.00 23.20 23.40 80 94 m/Z 94.05 11.59% 160 30 42 52 66 11 0 h1 ■" . ......... .. ] 111. TTHTt tt 108 118 ,. 132 . । 146 . rl, . 1791791 .,., mfa-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1(18

22.80 23.00 23.20 23.40 5000 m/z 80.10 10.73%

— 80 94 160 , , 17 30 42 52 66 , 108 118 132 146 ,|| 170179,i 0 TFTTTTI111111111111111111111111 p < Ftrr TTTu mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79802:2-Methyl-2,3-epoxy-2,3-dihydrc5-1,4-naphthoquinone 188 22.80 23.00 23.20 23.40 173 m/z 184.10 10.60% 5000 89 76 105 131 160

51 62 I 115 146 0---+— - - tW TTrr mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10980.D 050102.M Thu May 16 14:36:28 2002 Page 9

NYC-WTC_000023900

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NYC-WTC_000023900Source: NYC Law Department, mirrored locally

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