GCMS analysis results for sample AE11159, May 2002

NYC 9/11 Public Portal Document Llbrary search compound Report

Data File : C:\MSDCHEM\1\DATA\020515\11159.D Vial: 11 Acq On : 15 May 2002 9:42 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.31 ug/1 35120 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual ’ - --Ha gut— =e----------- 1 Phenanthrene-d10 188 C14D10 001517-22-2 72 2 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 50 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 45 4 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 42 Abundance Scan 4915 (31.958 min): 11159.D (-4904) (-) m/z 188.15 100.00% 188

5000

1 i r ■ ■ ■ I 1 ' 1 1 1 1 1 ' 1 1 1 1 1 1 1 1 94 158 44 54 66 78 | 132 146 ,i 170 । | 31.60 31.80 32.00 32.20 *mmmPmmmm**PDmmm m/z 189.15 13.99% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d 10 188

5000 —....... ....... "■T 31.60 31.80 32.00 32.20 80 m/z 94.25 13.77% 94 160 30 42 52 66 . 11 108118 132 146 , |,I 170179 " I ■1" I " " I"111" " 111" I 111" 11 " TTTTT n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79806: Naphthalene, 2,6-dimethoxy- 188 — 173 145 31,60 31.80 32.00 32.20 5000 rn/z 158.10 12.64% 102 28 114 130 TITTgoumuHt+197 7 H 15 39 51 63 75 88 mmmm m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79804: Naphthalene, 1,7-dimethoxy- 173 188 31.60 31.80 32.00 32.20 m/z 184.10 10.30%

5000 102 115 145

51 63 75 130 158 "." "."" i-'.1' r'1"' ii111' ।111 ."I'1.'I1". I'" 'i "'"i ""i1 |TT T’ -H /z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

11159.D SCAN020507.M Thu May 16 09:54:42 2002 Page 6

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