Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.
NYC-WTC_000048169–000048181Folder label: “GCMS X 4/9/02 A 4/19/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\020419\08426.D Vial: 13 Acq On : 19 Apr 2002 7:57 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 • *********************************************************************** Peak Number 5 Phenanthrene-diO Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.32 ug/1 692316 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Phenanthrene-diO 188 C14D10 001517-22-2 90 2 Anthracene-diO- 188 C14D10 001719-06-8 86 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 4 Pentacyclo[7.3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 38 Abundance Scan 4915 (31.958 min): 08426.D (-4905) (-) m/z 188.05 100.00% 168
5000
94
/z-> „rr .... 4049. 66 I i 132 80 158 „lt.— " i " 1' r ■1 'l11 "I' 111" ............ I......... .. I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20 m/z 94.10 17.75% Abundance #79827: Phenanthrene-d10 188
5000 ‘II ' 1 I ' 1 1 ' I ' ' ' ' I ' 31.60 31.80 32.00 32.20
80 94 m/z 189.10 15.56% 160 30 42 52 66 I 108118 132 ' i' "11" " I" " I" 11111" I'1111" 1' ' P*" I11 1 1 11,1' | 11 II | h M I I146, +.170179, I.., n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d IQ- 118
31.60 31.80 32.00 32.20 5000 m/z 184.10 15.32%
80 94 160 I. 66
m/z-> 17 30 42 52 ■ i1"11" ■' i" " 11" 1111' HH | .1 108 118 132 11"»111 ■ ■ I ■ ■" I ■ ■ ■ ■I'»■ Ttt 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 146—+4179179—— Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 31.60 31.80 32.00 32.20 m/z 80.10 12.19%
5000
143 . 89 115 | 64 76 J. 102 ! 130 I 158 170 n/z—> ' i' " ‘ i ‘ 51 ' r "' r 1 " I'" ' . । A . ।, I’ 111 H 11 ■ 11111111 therrr r, 11 + 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ■111"11 h'" i" I 31.60 31.80 32.00 32.20
08426.D SCAN020418.M Thu May 02 15:30:24 2002 Page 7
NYC-WTC_000048179
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NYC-WTC_000048195
Laboratory report documenting GCMS analysis of sample AE08428 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048182
Laboratory report documenting GCMS analysis of sample AE08427 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048121
Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048134
Laboratory report documenting GCMS analysis of sample AE08324 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048207
Laboratory report documenting GCMS analysis of sample AE08429 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048106
Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048623
Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048660
Laboratory report documenting GCMS analysis of sample AE08488 conducted on May 7, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048635
GC/MS analysis report for sample AE08486 conducted May 7, 2002, detecting unknown compounds and surrogate standard 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048647
Laboratory report documenting GCMS analysis of sample AE08486 conducted on May 7, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048672
Laboratory report documenting GCMS analysis of sample AE08489 conducted on May 7, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047886
GCMS analysis report for sample AE08256 showing surrogate recovery and unknown compounds from April 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000048081
Department of Environmental Protection GCMS analysis record dated April 9-19, 2002.
Filed in the same folder
NYC-WTC_000048082
Fragmented document page containing metadata and identifiers related to GCMS testing procedures from early April 2002.
Filed in the same folder
NYC-WTC_000048085
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank run (Sample AE08323) from April to May 2002.
Filed in the same folder
NYC-WTC_000048094
Laboratory report of GCMS calibration (Sample AE08323) conducted between April 9 and May 3, 2002, showing response factors for volatile organics.
Filed in the same folder
NYC-WTC_000048098
Laboratory report of GCMS reference standard run (Sample AE08323) conducted between April 9 and May 3, 2002, verifying instrument performance.
Filed in the same folder