GCMS analysis results for sample AE08323, May 2002

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Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048106–000048120

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08323.D Vial: 10 Acq On : 19 Apr 2002 4:59 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.35 ug/1 736473 Phenanthrene-dl 0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 80 2 Anthracene-dlO- 188 C14D10 001719-06-8 78 3 2-Isoxazoline, 3-mesityl-5-pheny... 297 C18H19NOS 1000164-78-1 36 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 36 Abundance Scan 4914 (31.952 min): 08323.D (-4906) (-) m/z 188.15 100.00% 188

5000

80 94 TTF i r - ■ 1 i - • - ' । « ‘tr । - 4° 66 | 31.60 31.80 32.00 32.20

n/z-> i-q-T - 20 40 60 +13214610.4 ‘ T‘111.1111111T10‘T111‘111117 80 100 120 140 160 180 200 220 240 260 280 300 m/z 184.10 18.57% Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 80 94 m/z 94.05 17.67% 160

m/z-> +30.5264 132146 | 108 ^'T' . ................. I ... - o 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79826: Anthracene-d10- 188 ‘I FT’’ i -r-( । । । । ^ । i । । । > 31.60 31.80 32.00 32.20 5000 m/z ,80.10 15.84%

„ 80 94 160

m/z-> 17,30,52%.44 20 118132146,|| । n’r '' »> | ' Moi । । |‘W 80 100 120 140 160 180 200 220 240 260 280 300 40 60 T‘l‘rt11111111"TTTVIEIIIITIT"T

Abundance #79743: 2-Isoxazoline, 3-mesityl-5-phenylthio- TTT 188 31.60 31.80 32.00 32.20 m/z 189.20 14.72% 5000 119 146 91 160

m/z—> .27 41, 63 77 194. ,122,11,1.174, ■ ■ i ■1 1 ■ I ■ ■ ■ ■ i ■ ■1 ■!' 202 237 254 269 297 ' ■ l ■ • ■ ' I 1 1 1 I | 1 1 1 1 e1 1 > 1 | > 1 < | 1 1 TTT i ' 1 'T i 1 1 1 1 I 1 1 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.60 31.80 32.00 32.20

08323.D SCAN020418 .M Thu May 02 15:23:57 2002 Page 8

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GCMS analysis results for sample AE08324, May 2002 · Box DEP Box 27

NYC-WTC_000048134

Laboratory report documenting GCMS analysis of sample AE08324 conducted on May 6, 2002, including surrogate recovery data.

1 shared topics · Same agency, volume and box · similarity 0.998