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GCMS analysis results for sample AE08323, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048106–000048120

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048116
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08323.D Vial: 10 Acq On : 19 Apr 2002 4:59 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 5H-Dibenzo[a,d]cycloheptene Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.28 ug/1 592748 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 50 2 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 40 3 6,2,5-Ethanylylidene-2H-cyclobut... 192 C11H12OS 019086-86-3 40 4 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 38 Abundance Scan 4767 (31.088 min): 08323.D (-4758) (-) m/z 192.05 100.00% 1912

5000

40

m/z-> i""rr . ............ . .. ......... 1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 IIT 30.80 31.00 31.20 31.40 m/ z 40.10 20.14% Abundance #80999: 5H-Dibenzo[a,d]cycloheptene 192

177 5000 30.80 31.00 31.20 31.40 89 165 m/z 191.10 18.24%

m/z—> 39 1*009000*000—""—- 76 , | ,102 115 128 139 152 51 63 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TITT 4 Abundance #80907: 2-Imidazolidinone, 1 -methoxy-3-phenyl- ' 106 19/2

77 162 30.80 31.00 31.20 31.40 119 m/z 193.10 15.57% 5000 42 56 91

/z—> pm HHt28 t .111,65.,.. H , । 134 1 | " ' । | " " I ' । ' I | । I I ! | I I I ! |l 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 " I'1 Abundance #80887: 6,2,5-Ethanylylidene-2H-cyclobuta[cd][2]benzothiop... 1 1 i 1 ' 1 ' i ' ■ 80 192 30.80 31.00 31.20 31.40 m/z 146.20 10.94%

5000 59 91 113 39 136 163

m/z—> 11ITTI1 |ll, , +ryaallll‘,I, 199 na. „ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I' * H l ‘ ‘II’ 111111111 4-— 30.80 31.00 31.20 31.40

08323.D SCAN020418.M Thu May 02 15:23:56 2002 Page 7

NYC-WTC_000048116

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NYC-WTC_000048116Source: NYC Law Department, mirrored locally

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