GCMS blank analysis results for sample AE08958, April-May 2002

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'Data File : C:\MSDCHEM\1\DATA\020424\0416LB.D Vial: 3 Acq On : 24 Apr 2002 11:44 am Operator: Nefliu Sample : 04/16 lab blk Inst : Instrumen Misc : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 5H-Dibenzo[a,d]cycloheptene Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.21 ug/1 651980 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 45 2 1H-Indene, 2,3-dihydro-2-methoxy... 224 C16H160 111864-82-5 42 3 9H-Fluorene, 9-ethylidene- 192 C15H12 007151-64-6 38 4 Benzoic acid, 3-formyl-6-hydroxy... 238 C12H1405 038629-36-6 36 Abundance Scan 4767 (31.088 min): 0416LB.D (-4759) (-) m/z 192.05 100.00% 192

5000 40 120 146 160 240 ■ mmm 30.80 31.00 31.20 31.40

miz-> 20 । ■1 451.66.4441,108 40 60 80 100 120 140 ■ ■ । 'I ■ " ‘ I " 160 180 -++ 200 220 240 m/z *vRRvRAywNw~ 40.10 23.16% Abundance #80999:5H-Dibenzo[a,d]cycloheptene 192

177 5000 30.80 31.00 31.20 31.40 89 165 m/z 191.10 21.33% 1***1* 39 51 63 1 1 76,44102 115 128139 122 .. T 1111 11 i1 111111 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #81106:1H-lndene, 2,3-dihydro-2-methoxy-1 -phenyl-, cis- 1112 224 30.80 31.00 31.20 31.40 5000 m/z 193.10 18.86% 179 165 115 26 39 51 63 77 -i -91 ! ■•! ■ । ‘["i' *ri [ v ■, A -i " । 103 | 128139 152 I 209 1 1)* 1 i mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #81028:9H-Fluorene, 9-ethylidene- 1 ' i 1 ■ • ■ i A• • । ■ ■ • • । 192 30.80 31.00 31.20 31.40 rn/z 146.10 13.11%

5000 165 99 83—

iz—> 20 41 40 60 80 100 1 ’ i • ’ * 1 i • • • • i • • • • i • * 120 140 160 180 200 j • i * r • * i • • 220 240 J. 4A.W 30.80 31.00 31.20 31.40

0416LB.D SCAN020424.M Thu May 02 14:37:22 2002 Page 5

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