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GCMS sample analysis results for AE10700, May 20 2002

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Laboratory report detailing GC/MS analysis of sample AE10700 including surrogate recovery data in May 2002.

NYC-WTC_000045735–000045747

Folder label: “GCMS X 5/3/02 A 5/13/02

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Scanned page image, NYC-WTC_000045744
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NYC 9/11 Public Portal Document ULJLCLY ocaiun UtpOulIU RCDOL L

Data File : C:\MSDCHEM\l\DATA\020513\10700.D Vial: 11 Acq On : 13 May 2002 10:25 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 5H-Dibenzo[a,d]cycloheptene Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.30 ug/1 31792 Phenanthrene-dl0 31.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 5H-Dihenzo [a, d] cycloheptene 192 C15H12 000256-81-5 45 2 1H-Indene, 2,3-dihydro-2-methoxy... 224 C16H160 111864-82-5 45 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 42 4 4-Hydroxy-3,5 - dirye thyl cinnamic acid 192 C11H1203 1000132-15-8 33 Abundance Scan 4768 (31.094 min): 10700.D (-4757) (-) m/z 192.10 100.00% / 192 /1

5000

TIInr 20 96 160 30.80 31.00 31.20 31.40 0 —54,, 70। 84 J 146 | 282 m/Z 193.20 —P— I | I I' I I | I J I I | I I — [ Fr I I J I I I 1 | PT ■ । ■ ■ ■ ■ t ■ ■ ■ ■ । । । । ।■ 20.68% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #80999: 5H-Dibenzo[a,d]cycloheptene 192

177 5000 1 1 I1 1 30.80 31.00 31.20 31.40 165 m/z 191.00 19.13% 89 152 | 39 51 63 76, | 102115128 , 4 । । h , — m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 1#81106:1H-lndene, 2,3-dihydro-2-methoxy-1-phenyl-, cis- 192 224 30.80 31.00 31.20 31.40 5000 m/ z 96.10 17.39% 179 165 115 26 39 51 63 7 91 193 127139152 ----- TT+-117—74 •' l 1 1 ' I 209 I I I I I I I I I i I I I I

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #125844: Anthracene, 2-methyl- 192 30.80 31.00 31.20 31.40 rn/z 159.90 14.78% 5000

„ 96 165 ............ I 1,1 1 1 115 6311,111 I ' ' 1 ' I 1 ‘TI 1 1 1 1 1 1 139151 1 11 1 1 1 1 I 11 I ' I I I ' i ■ ’ ■ 1 i 1 1 1 1 i 1 1 1 1 1 1 1 11 1 1 1 1 1 1 1 ' ' 1 1 11 1 I ' 1 ' 1 1 1 1 -n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 30.80 31.00 31.20 31.40

10700.D SCAN020507.M Wed May 15 08:39:47 2002 Page 6

NYC-WTC_000045744

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NYC-WTC_000045744Source: NYC Law Department, mirrored locally

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