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GCMS chain of custody form, sample AE10238, May 2002

Machine-extracted title · confidence 100%

Chain of custody record for GCMS analysis of sample AE10238 on May 20, 2002, including surrogate compound data.

NYC-WTC_000024412–000024422

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024418
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020509\10238.D Vial: 16 Acq On : 10 May 2002 1:27 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C: \MSDCHEM\1\METHODS\SCAN020507 .M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 5H-Dibenzo[a,d]cycloheptene Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.36 ug/1 53739 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5H-Dibenzo [a, d] cycloheptene 192 C15H12 000256-81-5 59 2 Phenanthrene, 4-methyl- 192 C15H12 000832-64-4 53 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 53 4 4-Hydyoxy-3,5-dimethylcinnamic acid 192 C11H12O3 1000132-15-8 50 Abundance 7 Scan 4768 (31.094 min): 10238.D (-4754) (-) m/z 192.10 100.00% 192

5000 ............................... 42 70 96 160 30.80 31.00 31.20 31.40 406 Tle+dp... ■ I ] A f f ■ > l ! < [■>IIJlI ■>Jl I ■1 |I ■I I| 1I II J!I >> | i" " i'1 ■ ■ i MTi 1uuu m/z 191.00 20.56% m/z—> 20 40 60 80 100120140160180 200 220 240 260280300 320 340360 380 400 Abundance #80999: 5H-Dibenzo[a,d]cycloheptene 192 f

5000 AA 30.80 31.00 31.20 31.40 165 m/z 193.10 16.30%

n/z—> Abundance - 39 63 89 115 139 L i"111'11 ■ i ■11111111111'1 r ■" r ■ ■ ■ r1" 20 40 60 80 100120140160180 200220 240 260 280300 320 340 360380400 #125851: Phenanthrene, 4-methyl- 192 ....................................... 30,80 31,00 31.20 31.40 5000 m/z 69.90 10.58%

40 95 165

nz-> 63 11’7 11211’7 42L Tp-rTiyrrrTp-rTTp-rTTp-rTTYTTTTp-rrTpT^^ 20 40 60 80 100120140160180 200220240 260280300 320 340360380400 Abundance #125848: Anthracene, 9-methyl- 192 30.80 31.00 31.20 31.40 m/z 96.20 10.01%

5000

39 63 .1115 139 165, TTTTTTTTTTAmpmh ' i ‘' i11" i" " i" " i" " i"'' l" " i'" ' i" " r'" i -AA- n/z—> 20 40 60 80 100120140160180200220240260280300 320340360380400 30.80 31.00 31.20 31.40

10238.D SCAN020507.M Tue May 14 14:24:49 2002 Page 4

NYC-WTC_000024418

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NYC-WTC_000024418Source: NYC Law Department, mirrored locally

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