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GCMS sample analysis results for AE10700, May 20 2002

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Laboratory report detailing GC/MS analysis of sample AE10700 including surrogate recovery data in May 2002.

NYC-WTC_000045735–000045747

Folder label: “GCMS X 5/3/02 A 5/13/02

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Scanned page image, NYC-WTC_000045745
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NYC 9/11 Public Portal Document DCCLil wpOul RCDUL L

Data File : C:\MSDCHEM\1\DATA\020513\10700.D Vial: 11 Acq On : 13 May 2002 10:25 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Phenanthrene-diO Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.35 ug/1 36510 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 72 2 2,6-Naphthoquinone, 1,5-diamino- 188 C10H8N2O2 002783-59-7 52 Anthracene-dl0- 188 C14D10 001719-06-8 50 4 Phosphonic acid, (3-methyl-3-pen... 188 C8H13O3P 022152-34-7 50 Abundance Scan 4914 (31.952 min): 10700.D (-4905) (-) m/z 188.10 100.00% 188

5000

66 80 94 ■ ■ i 1 ■ ■ ■ i ■ • ■ > I ■ ■ ■ ■ । । > ■ । । 1 . 160 31.60 31.80 32.00 32.20 T I I | I I I I | 1 1 52 ! I | — | . 115 , 141 1..... „ 1.213 ■ ■ । 1 ■ 1 ■ l ' 1 1 ' । 1 1 ■ i 1 1 1 1 i m/z 184.10 20.91% m/z->______ 20 40 60 80 100 120 140 160 180 200 Abundance #79827: Phenanthrene-d10 188

5000 ■ 1 । ' 11■i1 1 1 1 1 1 1 1 ।1 ■11' । 1 31.60 31.80 32.00 32.20 m/z 94.00 17.91% 80 94 160 +30,425,14 , Il 108118, 132 146, | 179, l , , I r ■ ■ ' i n/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #79755: 2,6-Naphthoquinone, 1,5-diamino- 188 ' ' I ' ' 1 ' I 1 1 1 1 I 1 ' 1 1 I ■’ 1 1 1 I ' 31.60 31.80 32.00 32.20 132 m/ z ,80.10 14.60% 5000 160 104 = 66 77 n/z-> ..28 20 38.51. 40 . 60 I.. . 80 TII 100 115 120 +145 140 1, 160 170 1 1 1 1 1 180 II ' ■ i ' 1 1 1 i 200 Abundance #79826: Anthracene-d10- 188 31 60 31.80 32.00 32.20 m/z 66.10 14.58%

5000

— 80 94 160 , I

Tl/Z--> 1720.42.52,6.1. 20 40 60 80 108118 132 146 Ur Tr ' ''I'1 100 120 1 1 140 ,1,179... 160 180 200 i 1 ■ 1 ’ i ■ ■ i ' 1 1y 0 31.60 31.80 32.00 32.20

10700.D SCAN020507 .M Wed May 15 08:39:47 2002 Page 7

NYC-WTC_000045745

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NYC-WTC_000045745Source: NYC Law Department, mirrored locally

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