GCMS chain of custody form, sample AE10210, May 2002

NYC 9/11 Public Portal Document *— 2

Data File C:\MSDCHEM\1\DATA\020509\10210.D Vial: 12 Acq On 9 May 2002 9:29 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.43 ug/1 53484 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Phenanthrene diO 188 C14D10 001517-22-2 81 V2 Ant acene-dlO- 188 C14D10 001719-06-8 43 3 3-/mino-4 -methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 4M[ethyl-2- (4-fluorophenyl)pyrim. . . 188 C11H9FN2 076128-67-1 37 Abundance Scan 4915 (31.958 min): 10210.D (-4903) (-) m/z 188.20 100.00% 188

5000

80 92 mo 160 31.60 31.80 32.00 32.20 49 66 I, 102 ‘T’’’ . p-r . > | > i I > । . TTTTTTTTTNTTTTHTTNTTTTTTTTTTTTT TT m/ z 80.10 22.86% n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 168

5000 31.60 31.80 32.00 32.20 m/ z 184.00 12.11% 80 94 160 30 42 52 66 . 11 108118 132 146 ,|,| 170179 TTWTTTTTTTTTTTTTTTHTTTTTTH 111 I. if I! np h । m 111 ! rr| i > t rp rlni 1 1'1 " 11 11 11 " 1 11 m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160170 180 190 Abundance #79826: Anthracene-d 10- 188

31.60 31.80 32.00 32.20 5000 m/z .92.00 11.71%

80 94 17 30 42 52 TPPPTTT 66 # 108 118 ' 'I ।' ।' I" '' l' 132,146 14 7o1z l. TT miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 31.60 31.80 32.00 32.20 m/z 189.10 11.00% 145 5000

117 , 159 173 Tp4 41 51 63 77 89 102 130

m/z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10210.D SCAN020507.M Tue May 14 14:23:22 2002 Page 7

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