GCMS analysis results for sample AE08963, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08963 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049609–000049621

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

• Data File : C:\MSDCHEM\l\DATA\020424\08963.D Vial: 14 Acq On : 24 Apr 2002 10:39 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.37 ug/1 724832 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-diO 188 C14D10 001517-22-2 78 2 Anthracene-dlO- 188 C14D10 001719-06-8 50 3 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 50 4 Antipyrine 188 C11H12N2O 000060-80-0 50 Abundance Scan 4914 (31.952 min): 08963.D (-4901) (-) m/z 188.20 100.00% 188

5000

80 TTT 1***I**’’I’’I’ 94 158 । 31.60 31.80 32.00 32.20

miz-> ImPmmptbpH 41 54 66 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 -132.146.4.179,..‘I m/z 80.15 16.86% Abundance #79827: Phenanthrene-d10 188

— 5000 TTT i ' ■ ■ ■ i ■ ■ ■ ■ i • 31.60 31.80 32.00 32.20 m/z 189.20 16.51% 80 94 160 30 42 52 P .1 ,| 108118 132 146 d 170179.1,1 | . ! .. . . (. > ,. |. ■ 11 ,, , | 11 L . | (I I . j., 11 I I H 11 [ I > ■ 111 I 11 11 ,1 | i l-n-j+11 I | I 11 11 I ITl'I'l I I I | I I 11 J I'I'I'I1] I > I ’T niz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188 f 31.60 31.80 32.00 32.20 5000 m/z94.10 13.07%

80 94 160 , 17 30 42 52 P . ,| 108118 132 146 I. 170179.1.1 l । ,. ., ।.... j. , . ■ j l .. >! 111 .1111. ।.. 1111 ,11 ] 11.. | 11 I 11 111111111 | lu 1111111111 Hi 11111 111 Jl’l’l’ 111 TT miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79744:4-Methyl-2-(3-fluorophenyl)pyrimidine —rT . . ) । . ,T| I i | 1 | ri i i । r 18 8 31.60 31.80 32.00 32.20 m/z 184.10 12.36% 5000 121

173 67 94

/z—> 39 50 mmTLmPTTTT | , 82 |, 108 | j i....... ■ ri ■ • ■ ■ । 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 1«) 170 180 190 +134,146 11 4 J \ ________________ ’*I**’*I4*+’I4’ I’41) 31.60 31.80 32.00 32.20

08963.D SCAN020424.M Thu May 02 14:52:42 2002 Page 8

NYC-WTC_000049620

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GCMS analysis results for sample AE08960, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049571

Laboratory report documenting GCMS analysis of sample AE08960 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998