GCMS analysis results for sample AE08961, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08961 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049584–000049595

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

-Data File : C:\MSDCHEM\1\DATA\020424\08961.D Vial: 12 Acq On : 24 Apr 2002 8:41 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Phenanthrene, 1-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.32 ug/1 630511 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 59 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 59 4 5-Isoindolinecarboxylic acid, 1,. . . 317 C18H23NO4 033975-34-7 50 Abundance Scan 4767 (31.088 min): 08961 .D (-4755) (-) m/z 192.10 100.00% 192

5000 40 ■ ■ i ■ ‘ 30.80 31.00 31.20 31.40 49 8226109118132 146 160 Tppt mmPmTmmmmmp Hprr m/z MARRwWNWWWA 40.10 23.03% iz-> 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 200 Abundance #125856: Phenanthrene, 1-methyl- 192

5000 30.80 31.00 31.20 31.40 m/z 193.20 17.14% 96 IRK 27 39 51 63 82 l 115 126 139 152 190 178 ।.... l,.,. i p . m । r... । ThmmnmmmmmpsH ’t Tpu niz-> 20 30 40 50 60 70 80 90 100110120 130140 150160 170 180190 200 Abundance #81033: Phenanthrene, 9-methyl- 19/2 -r-r-p-TT-r-p-r-r-r-pr-r-r-r-p-r 30.80 31.00 31.20 31.40 5000' m/z 96.20 12.99%

96 icr 29 39 51 63 74 83 , a 115 126 139 152 j 176 J, | j i r» i । V Ih"j ¥ tUgs i I II’s * * I ITphrtpli rp IIt in 1111111.111*| 1111 p 1111 Plh 111 r 111 i’tpnr “i" n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- A T • ‘ • I * ‘ ' 1 T 192 30.80 31.00 31.20 31.40 m/z 191.10 11.79% 5000

86 27 39 51 63 82 ,ll 115 126 139 152 Y 176 „ 1 "■'i-'-■T"11 f ■ '■ I i‘i 1111 it -HTTWTTTTITTTTMTT Wp-r • ■ i ■ ' ■ ■ i < » n/z-> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

08961.D SCAN020424.M Thu May 02 14:46:09 2002 Page 6

NYC-WTC_000049593

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GCMS analysis results for sample AE08963, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049609

Laboratory report documenting GCMS analysis of sample AE08963 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998