GCMS analysis results for sample AE08961, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08961 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049584–000049595

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

• Data File : C:\MSDCHEM\1\DATA\020424\08961.D Vial: 12 Acq On : 24 Apr 2002 8:41 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 5-Oxazolecarboxamide, 2-phe... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.29 ug/1 569869 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5-Oxazolecarboxamide, 2-phenyl- 188 C10H8N2O2 039819-42-6 43 2 Anthracene-dlO- 188 C14D10 001719-06-8 43 3 Phenanthrene-diO 188 C14D10 001517-22-2 38 4 Antipyrine■ 188 C11H12N20 000060-80-0 37 Abundance Scan 4915 (31.958 min): 08961 .D (-4899) (-) m/z 188.15 100.00% 188

5000 94 1*mnmnmmn/.m 40 80 it 31.60 31.80 32.00 32.20 • i ■ ■ ■ ‘ i1 •1 ■ i • “ ■ --FHH 57 66 132 146 160 1111111. i > n 11 >>-[>■ > f l 1111" । ■ > 11 ■ n । I'M1 T m/z 94.20 25.50% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79737:5-Oxazolecarboxamide, 2-phenyl- 116 188 144

5000 TI --------- 31.60 31.80 32.00 32.20 89 m/z 189.20 22.10% 28 39 51 63 77 105 1 ’1l.......................... ' i • ■ ■ • i • ■ t 11 ■ i’i 1111 |'i ■ ■ 111'i 11111 i'i 1111l 111 THp IITTEETIT 41’1**1***12+4*41*44 i1 “■ i nz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 ‘ P ’ ' 1 ] ‘ ■ IT , • 1 I 1 | > । I 1 , I 31.60 31.80 32.00 32.20 5000 m/z 40.10 17.61%

RR 80 94 160 1 17 30 42 52 P „ 108118 132 146 'i 111 ■ 11.. n j 11. i, I,. 1111111 i-l 111111111.11 [ 11,1111: i, 11 r 11 u . i, 1111 p-rl-r,. tl’ II 170179., r’l’lt •m-n niz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 *I***’A’*I**1TII’l 188 31.60 31.80 32.00 32.20 m/z 80.05 16.86%

5000

80 94 160 30 42 52 66 n/z—> TpHTHHt- ....................................... .*****)***** 1 108118 132 146 J 1701791,1 10 2030405060 70 8090 100110120130140150160 170 180 190 1’1 mera 31.60 31.80 32.00 32.20

08961.D SCAN020424.M Thu May 02 14:46:11 2002 Page 7

NYC-WTC_000049594

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GCMS analysis results for sample AE08963, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049609

Laboratory report documenting GCMS analysis of sample AE08963 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998