GCMS analysis results for sample AE10023, May 2002

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- Data File C:\MSDCHEM\1\DATA\020507\10023.D Vial: 22 Acq On 8 May 2002 8:49 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.33 ug/1 38814 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthfacene-d10 - 188 C14D10 001719-06-8 53 2 Pentacyclo[8.4.0.0(3,7) .0 (4,14) . . . . 188 C14H20 1000099-27-2 37 3 Phenanthrene -d10 188 C14D10 001517-22-2 33 4 Nii el) di-.mu.-carbonylbis(.eta... 302 C12H10Ni2O2 012170-92-2 23 Abundance Scan 4915 (31.958 min): 10023.D (-4904) (-) m/z 188.10 100.00% 188

5000 94 ,................... 80 158 42 66 132 31.60 31.80 32.00 32.20 ..... 4.... I ..........1...... 1 ■ ■।> r■■11■■11■■■111 266 ‘TT 1 1*1090110001000010BBOim 297311 m/ z 94.00 33.41% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79826: Anthracene-d10- 188

5000 U.............. ■ | T ■ 1 ' | ‘ 1 ■ • | ' 1 । | । । ‘ | । 31.60 31.80 32.00 32.20 m/z 189.20 33.15% 30 52 66 J J — 80 94 118132146 160 TI—uuptntuut.——mp—tper T1nn, r 1 ' 1 I 1111 11 ■1 1 ' I mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79714: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11 )]tetradecane 188 0*/*/ 31.60 31.80 32.00 32.20 5000 m/z 184.20 20.68% 91 117131 145159173

miz—> 20 —27155 4444 ’ ’I’’’’ T1 ■1 1 i 1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 /................................... Abundance #79827: Phenanthrene-d10 1 1 ' 1 ‘ tyr ’11 r-r-i i -[ i i i । । i 188 31.60 31.80 32.00 32.20 m/z 80.00 16.41%

5000

80 94 160 ,39,152/66.1 | 108 132146 ,|I 1,1111'""' I " । ' i *1 n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.60 31.80 32.00 32.20 |

10023.D SCAN020507.M Tue May 14 08:45:38 2002 Page 7

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