GCMS analysis results for sample AE10025, May 2002

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Laboratory report documenting GCMS analysis of sample AE10025 conducted on May 14, 2002, identifying unknown compounds.

NYC-WTC_000044191–000044202

Folder label: “GCMS X 4/26/02 A 5/8/02”

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NYC 9/11 Public Portal Document

• Data File C:\MSDCHEM\l\DATA\020507\10025.D Vial: 24 Acq On 8 May 2002 10:47 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.35 ug/1 43989 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene -dlO- 188 C14D10 001719-06-8 86 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Berzene, 1-(1-cyclohexen-l-yl)-4 . . . 188 C13H160 020758-60-5 45 4 Benzaldehyde, 2,5-difluoro-4-hyd... 188 C8H6F2O3 148872-77-9 40 Abundance Scan 4914 (31.952 min): 10025.D (-4906) (-) m/z 188.15 100.00% 188

5000

1 ■ I r . ' y( . 1 -I I I I ! 1 | I I > , | , 94 160 31.60 31.80 32.00 32.20 43 76 I 112130 ,l 207 266 345 ......... |’*i TPTp m/z 189.15 16.26% /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79826: Anthracene-d10- 188

5000 » * I t ■ ' r ■^ । 1 ' ■ ■ । ■ ■ ■ ■ । ■

31.60 31.80 32.00 32.20 m/z 94.10 12.74% 66 , 94 160 L

n/z-> 1720—42*4141324 I ■'1111''11'1'' I''111111' 111 r'I'1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79827: Phenanthrene-d10 188 P1 Pr । । । । । । । । । । , 31.60 31.80 32.00 32.20 5000 m/ z 160.00 12.42%

80 160

m/z-> 30 T’’0’E707 20 40 SU 44001324 111 ■ ■ ‘' i ■ "' i ■ ■ ■' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■'' i ■ ■ 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79791: Benzene, 1-(1-cyclohexen-1-yl)-4-methoxy- 188 31.60 31.80 32.00 32.20 m/z 80.10 10.74%

5000 160

91 129 51 m/z-> 111"1111,41 4, 75.4198444. Tit 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 11 " 11 " 111 TTT i ‘ r ' 1 i ri 1 1 1 1 1 1 1 1 1 31.60 31.80 32.00 32.20

10025.D SCAN020507.M Tue May 14 08:46:23 2002 Page 7

NYC-WTC_000044201

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NYC-WTC_000044203

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