GCMS analysis results for sample AE10021, May 2002

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• Data File C:\MSDCHEM\1\DATA\020507\10021.D Vial: 20 Acq On 8 May 2002 6:51 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

31.95 0.37 ug/1 47744 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10 - 188 C14D10 001719-06-8 50 2 Phenanthrene-diO 188 C14D10 001517-22-2 50 3 4/Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 40 4 /,4-Naphthalenedione, 2-hydroxy-... 188 C11H8O3 000483-55-6 40 Abundance Scan 4913 (31.946 min): 10021.D (-4906) (-) m/z 188.20 100.00% US

5000

94 1‘I‘‘II*‘II4IIII‘III 31.60 31.80 32.00 32.20 1111 ■ ■ i" 1' i 43 66 80 MI mmt i| 1111 j111111 103..... 132.... 158170 180 m/z 189.20 21.96% mfe-> W 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- US

5000 31.60 31.80 32.00 32.20 m/z 93.90 18.56% 80 94 160 , |.

n/z-> 17 30 42 52 66 ' i " '11''111" " I" " *fTrr"i ।' । + ,1 108118 11' 11" " ।। 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132 " 1111 ,146.4.179179/ Abundance #79827: Phenanthrene-d10 US < > I ’ ■ ■ -1 ■ ■ ■ i । ■ > । 1 > I > < । < I । 31.60 31.80 32.00 32.20 5000 m/z 158.10 8.60%

80 94 160 30 42 52 66 , 11 108118 132 146 II 170179,1,1 11" " i11111" " |1"1 ttrrrti 111 • 1-111 > i t 111111111TTT i 11111 [ 11111111111 "I’l’’ 111,11111 i'l'llll| । n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79745:4-Methyl-2-(4-fluorophenyl)pyrimidine 1 ‘ i 1 ' ‘ 1 1 1 1 1 I 1 1 1 ' I 1 1 1 1 1 1 US 31.60 31.80 32.00 32.20 m/z 79.95 8.33% 121 5000 173 67 94 39 57 | 133 146 161 84 |( .....I 111" ■ i "111" 1 ■ i'1" r "11" 111' i " " 1111111111 F’Ti11 " i" " i " i'11"111" " 11 ' 11" ■1 T’T T’F i > > ■ ■ । ■ ■ ■ < । । ■ > ■ । ■ n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10021.D SCAN020507.M Tue May 14 08:44:57 2002 Page 7

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