GCMS analysis results for sample AE10061, May 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\020507\10061.D Vial: 25 Acq On 8 May 2002 11:46 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.35 ug/1 37592 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 3 -Amino-4 -methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 59 4 4 H-Pyrido[1,2-a]pyrimidin-4-one,... 188 C11H12N2O 057773-19-0 53 Abundalince Scan 4914 (31.952 min): 10061.D (-4903) (-) m/z 188.10 100.00% 188

5000 --

' ■ ■ 1 52.80 i 1 1 1 ' i 1 ■ 136 1601 ■ 1 i 1 ' 1“ i 1 ■ ■ 1 i ' 1 I 1 1 1 1 I 1 1 1 1 i 1 ' 1 1 i ■ 448 31.60 31.80 32.00 32.20 m/z 189.30 12.42% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #79826: Anthracene-d10- 188

5000 TTF 1xddnn—n——B—n——T 31.60 31.80 32.00 32.20 m/z 187.10 11.51% 17 42 66.4% 132 16° ,1 , . n/z-> 50 100 150 200 250 300 350 400 450 Abundance #79827: Phenanthrene-d10 108 ■ ■ । 1 ' ■ ' i ' 1 ' 1 i 1 1 1 1 i 1 1 1 ' । 1 31.60 31.80 32.00 32.20 5000 m/z 80.05 11.20%

80 160 30 52. 100 132 1l i 1,1/d 1 ."1 r ■। । i i i । t i m—।—i—i—r m/z-> 50 100 150 200 250 300 350 400 450 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 009/01 31.60 31.80 32.00 32.20 rn/z 184.10 7.76% 145 5000

89 117

Tl/Z-> , . ,**,4 41 63

50 + —L1 ।

100 150 200 ■ i ' ■ ■ ■ । ■ 250 300 ■ ■ ' । 350 । । l 1 400 > 1 1 I > 450 ,.................................. 31.60 31.80 32.00 32.20

10061.D SCAN020507.M Tue May 14 08:46:47 2002 Page 7

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