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GCMS blank analysis results for sample AE10207, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis for sample AE10207 on May 14, 2002, listing compounds below method detection limits.

NYC-WTC_000024286–000024295

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024293
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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\020509\0501LBl.D Vial: 3 Acq On 9 May 2002 1:37 pm Operator: Nefliu Sample 05/01 lab blk kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Anthracene-diO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.32 ug/1 50647 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO-^ 188 C14D10 001719-06-8 78 ----- 2 Phenanthrene-d10 188 C14D10 001517-22-2 78 3 Pontae ±o[7.3.1.1. (4,12) . 0 (2,7) . . . 188 C14H20 1000215-61-8 50 4 2-Ouin tuecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 36 Abundance Scan 4913 (31.946 min): 0501LB1 .D (-4906) (-) m/z 188.15 100.00%l KB

5000

94 42 52 66 78 122 136 160 31.60 31.80 32.00 32.20 -------- TTTTPTT] T’T m/z 189.20 19.33%| mlz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- KB

5000 31.60 31.80 32.00 32.20 15.85%| 66 80 94 160 17 30 42 52 108 118 132 146 ,|.| 1701791, 11■" 1111■ 11■ ■■ ■ ।"11111: PH TTNTTTTHt TTnr iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 KB 1 ■ i ■ ■ ■ ■ i 1 1 11 i 1 31.60 31.80 32.00 32.20 5000 m/z 184.10 11.65%|

80 94 160 30 42 52 66 TIWWIPWOTTTTTTTTTH 4108118.132.146,4,179179... mz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )tetradeca... /...................... 1 ' I ‘ ’ 1 1 1 1 ' T । I I I I | | | I | | | KB 31.60 31.80 32.00 32.20 m/z 66.10 10.65% 5000 79 91 55 67 105 131 190 117 m/z—> ...... ...... I— ‘ 11 “ 11'; 111 ‘ “ I " " 1’’ ' l ‘ 145 1 158173..L " '11"11in' i111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

0501LB1.D SCAN020507.M Tue May 14 15:01:58 2002 Page 5

NYC-WTC_000024293

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NYC-WTC_000024293Source: NYC Law Department, mirrored locally

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