Laboratory report documenting GCMS analysis of sample AE10025 conducted on May 14, 2002, identifying unknown compounds.
NYC-WTC_000044191–000044202Folder label: “GCMS X 4/26/02 A 5/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
’ Data File C:\MSDCHEM\l\DATA\020507\10025.D Vial: 24 Acq On 8 May 2002 10:47 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 cis-2-Methyl-4-phenylthiane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.08 0.29 ug/1 36290 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 cis-2-Methyl-4/phenylthiane 192 C12H16S 076097-69-3 50 2 Thiophene, 2-[2- (3-thienyl)ethen... 192 C10H8S2 116854-09-2 42 3 3-(2-Methoxy-b-methylphenyl)acry... 192 C11H1203 103986-76-1 40 4 Thiazole, 2-/phenylthio) -___________ 193 C9H7NS2 033342-67-5 40 Abundance / Scan 4765 (31.076 min): 10025.D (-4759) (-) m/z 192.15 100.00% 192
5000
RA 62 96 146 160 30.80 31.00 31.20 31.40 41 50 ' r ' ■111 ■'11'1’' ■ ■ | .il l , 1111111''' 11'' ।। 114 111 " ■ 11111 r " 11 -H TT ejus m/z 193.10 21.06% n/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80922: cis-2-Methyl-4-phenylthiane ft 192
131 5000 91 117 143 30.80 31.00 31.20 31.40 104 163 m/ Z 96.10 18.66% 51 61 77 — „l 4lllq4L,, 177 1 ''111I 11' "'i 1111' I1 - n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 * Abundance #81023: Thiophene, 2-[2-(3-thienyl)ethenyl]- 1 2 . ......... 4.)A ........... 147 30.80 31.00 31.20 31.40 5000 m/z 160.10 14.58% 45
27 I 58 691 134 ao 96I A gt 115I 158 177 L WW (
11 " " I " 1,1111'' -----++++199+4 H i1'111' ■ * ip 111 [’ । > । [ । /z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid 192 . .... 1.1.4..... 161 30.80 31.00 31.20 31.40 m/ Z 82.20 14.39% 5000 105 77 132 91 115 145 39 51 65 rp .... d/moipnijaha 7 ,. ll ।. mmml—r X "."I.... . 11111" " I TTTT ' ' I 1 ' 1 1 I ' igi rj /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40
10025.D SCAN020507 .M Tue May 14 08:46:21 2002 Page 6
NYC-WTC_000044200
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NYC-WTC_000044203
Laboratory report documenting GCMS analysis of sample AE10061 conducted on May 14, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044132
Laboratory report documenting GCMS analysis of sample AE10020 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044144
Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044119
Laboratory report documenting GCMS analysis of sample AE10019 conducted on May 14, 2002, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044179
Laboratory report documenting GCMS analysis of sample AE10024 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044166
Laboratory report documenting GCMS analysis of sample AE10023 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044227
Laboratory report documenting GCMS analysis of sample AE10067 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044215
Laboratory report documenting GCMS analysis of sample AE10066 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044156
Laboratory report documenting GCMS analysis of sample AE10022 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024345
Chain of custody record for GCMS analysis of sample AE10210 on May 20, 2002, including surrogate compound data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024333
Laboratory report detailing GCMS analysis of sample AE10209 conducted on May 20, 2002, including surrogate recovery data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024402
Chain of custody record for GCMS analysis of sample AE10239 on May 20, 2002, including surrogate compound data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044098
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 26 and May 8, 2002.
Filed in the same folder
NYC-WTC_000044099
Fragmented page from a GCMS record series dated between late April and early May 2002 regarding environmental sampling analysis.
Filed in the same folder
NYC-WTC_000044100
Laboratory blank report for sample AE10019 showing non-detectable levels of target compounds from May 7, 2002.
Filed in the same folder
NYC-WTC_000044107
Laboratory report showing blank analysis results for sample AE10019 conducted between April and May 2002 with no detected contaminants.
Filed in the same folder
NYC-WTC_000044111
Reference report listing expected values for organic compounds including nitrosamines and chlorobenzenes used to validate analytical results.
Filed in the same folder