GCMS sample analysis results for AE10699, May 20 2002

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Laboratory report detailing GC/MS analysis of sample AE10699 including surrogate recovery data in May 2002.

NYC-WTC_000045721–000045734

Folder label: “GCMS X 5/3/02 A 5/13/02”

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NYC 9/11 Public Portal Document

• Data File : C:\MSDCHEM\1\DATA\020513\10699.D Vial: 10 Acq On : 13 May 2002 9:25 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Thiocyanic acid, 2-benzothi... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

31.08 0.34 ug/1 42440 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 38 2 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N6O 000945-24-4 38 3 3,4-Methylenedioxycinnamic acid 192 C1OH804 002373-80-0 38 4 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 28 Abundance Scan 4766 (31.082 min): 10699.D (-4755) (-) m/z 192.10 100.00% 192

5000

82 96 ..... J.... . 30.80 31.00 31.20 31.40 44 66 111 146 160 ----------- lal,, ‘I |I m" ' ' I 1 1 1 । I h । > '| । । । > । । । It 123 m/z 96.00 19.91% m/z->_____ 0 20 40 60 80 100 120 140 160 180 200 220 240 Abundance i#80870: Thiocyanic acid, 2-benzothiazolyl ester 192

5000 1 30.80 31.00 31.20 31.40 m/ Z 82.00 15.03%

n/z-> ....... 45.15/,80 108,122124 ......... । ■1 ■ 1 ।1 11 ■ ।1 1 ■11'' ■ 11 1 1 1 1 ।'1 ■ ■ । ■ ■ 111 0 20 40 60 80 100 120 140 1 i i 160 । 111 180 200 220 240 Abundance #80958:2,4-Diamino-6-(hydroxymethyl)pteridine 43 163 192 1 • ' । 1 ■ 1 ■ । 1 ■ ' i ' ' ■ ‘ i ‘ 1 30.80 31.00 31.20 31.40 5000 m/z 191.00 13.19% 28 68 . 146 176 92 106 121 133 |

n/z-> 0 i 1 1 1 ■ i 1 20 11,448,52. . LL. 40 60 80 100 120 140 160 180 200 220 240 Abundance #81021:3,4-Methylenedioxycinnamic acid 192 30.80 31.00 31.20 31.40 m/z 146.10 10.72% 5000

63 89 145 175

n/z-> 4.28 39,51 1 7 77 105 117 134 163 I I I ' I I I I I I I I I ’ I r I Ith—dlr. I I1' I I T "h, ' I—— ——————

0 20 40 60 80 100 120 140 160 I....................... ■ i ■ ■ ' 1 i 1 ■ 1 ■ I ' 180 200 220 240 . ....n___ 30.80 31.00 31.20 31.40

10699.D SCAN020507.M Wed May 15 08:36:13 2002 Page 7

NYC-WTC_000045731

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GCMS sample analysis results for AE10698, May 20 2002 · Box DEP Box 25

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Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.

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