Laboratory report documenting GCMS analysis of sample AE10019 conducted on May 14, 2002, identifying unknown compounds.
NYC-WTC_000044119–000044131Folder label: “GCMS X 4/26/02 A 5/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
’ Data File C:\MSDCHEM\1\DATA\020507\10019.D Vial: 18 Acq On 8 May 2002 4:53 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 6 Phenanthrene-diO Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T. 31.95 0.29 ug/1 30665 Phenanthrene-dl0 31.72
Hit# Of 5 Tentative ID MW MolForm CAS# Qual J 1 Phenanthrene-diO 188 C14D10 001517-22-2 59 2 Ant racene-d10- 188 C14D10 001719-06-8 45 3 4-M thyl-2-(4-fluorophenyl)pyrim. .. 188 C11H9FN2 076128-67-1 45 4 3-A ano-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 4913 (31.946 min): 10019.D (-4905) (-) m/z 188.20 100.00% 188
5000 — I ■ I ‘T | ■ I > 1 | I 1 I I ] I
41 । ----- 66 92 405 31.60 31.80 32.00 32.20 DT i ' । | । । । > | > i > .| I . . J | I H I | I H I | rr I | I I I I | I I I I | I I U [ / I'l I m/z 189.20 18.76% m/z—> 20 40 60 80 100120140160180200 220240260280300320340360380400 Abundance #79827: Phenanthrene-d10 188
5000 ‘ 1111111‘‘1I+‘‘II‘+II 31.60 31.80 32.00 32.20 80 m/ z 92.10 17.73% 160
m/z-> 30 52 TTImmmt 192.132.4... 4, 11t1‘11"T"CE"IIUP0—EI1——111U11TT 20 40 60 80 100120140160180200220240260280300320 340360380400 Abundance #79826: Anthracene-d10- 188
31.60 31.80 32.00 32.20 5000 m/ z 94.10 15.32%
RR 94 160
m/z—> -17.+42.664114132.44. " i"111" "i" " r 1" i ‘1" i T‘' " l 1‘1‘ . | l .TT 20 40 60 80 100120140160180200220240260280300320340360380400 Abundance #79745: 4-Methyl-2-(4-fluorophenyl)pyrimidine 188 31.60 31.80 32.00 32.20 m/z 160.00 13.00% 121 5000
67 94 39 ............ I .... 1.... 146 163 "11"1 'i"111n " i1111111" i,rTl i|T" P1" r1" r H 11111 • i111111'1111111111" I 1 ’ | r > • ’ I » ' ' k | • 1 ’ 1 | I « > > | T n/z-> 20 40 60 80 100120140160180200220240 260280 300 320 340 360 380 400 I 31.60 31.80 32.00 32.20
10019.D SCAN020507.M Tue May 14 08:39:43 2002 Page 8
NYC-WTC_000044130
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NYC-WTC_000044144
Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044191
Laboratory report documenting GCMS analysis of sample AE10025 conducted on May 14, 2002, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044203
Laboratory report documenting GCMS analysis of sample AE10061 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044166
Laboratory report documenting GCMS analysis of sample AE10023 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044132
Laboratory report documenting GCMS analysis of sample AE10020 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044179
Laboratory report documenting GCMS analysis of sample AE10024 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044215
Laboratory report documenting GCMS analysis of sample AE10066 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045811
Gas chromatography-mass spectrometry report for sample AE10705 showing detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044227
Laboratory report documenting GCMS analysis of sample AE10067 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044156
Laboratory report documenting GCMS analysis of sample AE10022 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024333
Laboratory report detailing GCMS analysis of sample AE10209 conducted on May 20, 2002, including surrogate recovery data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024345
Chain of custody record for GCMS analysis of sample AE10210 on May 20, 2002, including surrogate compound data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044098
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 26 and May 8, 2002.
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NYC-WTC_000044100
Laboratory blank report for sample AE10019 showing non-detectable levels of target compounds from May 7, 2002.
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Reference report listing expected values for organic compounds including nitrosamines and chlorobenzenes used to validate analytical results.
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