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GCMS analysis results for sample AE10019, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE10019 conducted on May 14, 2002, identifying unknown compounds.

NYC-WTC_000044119–000044131

Folder label: “GCMS X 4/26/02 A 5/8/02

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\020507\10019.D Vial: 18 Acq On 8 May 2002 4:53 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Anthracene, 1-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.35 ug/1 36756 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene, 1-methyl- 192 C15H12 000610-48-0 50 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 50 3 Naphtho [2 ,/3 -b] norbornadiene 192 C15H12 1000210-52-3 47 4 4-Hydroxy/3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 42 Abundance Scan 4767 (31.088 min): 10019.D (-4755) (-) m/z 192.20 100.00% 1912

5000

T_ -----

43 56 70 82 8 120 133 146 160 । 30.80 31.00 31.20 31.40 —PTTHTmmmmmmm 1' i11 m/z 96.00 13.60% n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160 170 180190 200 Abundance #125854: Anthracene, 1-methyl- 192

5000 30.80 31.00 31.20 31.40 m/z 82.20 13.27% 82 94 165

m/z-> 18 27 39 51 63 | 1. 115 126 139 150 | 176 ' | । > । i ]i i ii | f i r i'[ i i > i |’l r i t | i'l > i'i i I'l'r Ttl‘ I I I 1'] I I t 1 |Tl‘l I | I I F| | I | rI‘ I I I I |'I I I I | ill I [ mtrr l JI

10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 , k Abundance #81032: Phenanthrene, 2-methyl- 192 ,1....... 30.80 31.00 31.20 31.40 5000 m/ z 146.20 11.54%

83 95 165 28 39 50 63 74 I. I 115 126 139 150 J 176 . I I I > I I I I ■>'I I 1 I I iI I I I I TTTi I I I I I I I Pl I I II I I'l I I I I'l I f I I I > 1I I I I I I > i I I I TTTI 1 1 1 I ' ' ' 1 1 1 ' l 1 1 1 1 1‘ 111'' /z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #81026: Naphtho[2,3-b]norbornadiene 192 30.80 31,00 31.20 31.40 m/z 191.10 11.39%

5000 165

n/z-> 39 51 63 73 82 96 105 115 126 139 152 1 ''i ” <' «• J * ‘Ituu ! I1' l,'T' 11 H 11 "ri 11» m j 11 ri’i 111 FT'* I Tp-rrq-rTTT-]-

10 20 30 40 50 60 70 80 90 100110120130140150160 170 180 190 200 '" ।11 176.! 1 ' । ’ 1 1 ' । 1 30.80 31.00 31.20 31.40

10019.D SCAN020507.M Tue May 14 08:39:42 2002 Page 7

NYC-WTC_000044129

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NYC-WTC_000044129Source: NYC Law Department, mirrored locally

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