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GCMS analysis results for sample AE10209, May 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10209 conducted on May 20, 2002, including surrogate recovery data.

NYC-WTC_000024333–000024344

Folder label: “GCMS X 5/1/02 A 5/9/02

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NYC 9/11 Public Portal Document

• Data File C:\MSDCHEM\1\DATA\020509\10209.D Vial: 11 Acq On 9 May 2002 8:30 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Anthracene, 2-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.32 ug/1 40137 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 64 2 Anthracene, 1-methyl- 192 C15H12 000610-48-0 59 3 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 45 4 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 45 Abundance Scan 4768 (31.094 min): 10209.D (-4757) (-) m/z 192.10 100.00% 192

5000

1 ' i ■ ' ' ■ i ' ■ ' ■1 ' i ■ ■

40 49 66 8226 —THHHmmmmmmm 122 146 160 1 30.80 31.00 31.20 31.40 m/z 146.10 TT 14.67% mfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #81034: Anthracene, 2-methyl- 19/2

5000 ... M 30.80 31.00 31.20 31.40

82 96 165 m/z 96.20 14.24% 18 27 39 51 69 | II 115 126 139 152 J 176 „ " r1'11" i" "'l ■ ‘111'" " 11 ri 1111’r 111 I’ll ' 11 i‘i 1111 Tr’T7’ । r> 11111'| r, ■ r’h 11 pi 11111 ri 1111 ill ‘It ■n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance #125854: Anthracene, 1-methyl- 192 M...... ' 1 f1 1 1 1 I 1 1 ■ ■ i > ■ ■ ■ i ■ ■ 30.80 31.00 31.20 31.40 5000 m/Z 191.10 12.67%

82 94 165

niz-> 18 27 39 51 63 | h 115 126 139 150 I 176 „ TTTHTTTTTTTTTTTTTTTTTTTTTTHTTHIT , 1111.... I I'i'n-|ri !■! I I in'i I I i r’’ 11 1111!1! 11 i r»-i j 11 "’I 10 20 30 40 50 60 70 80 90 100110120130140150 160170180190200 U Abundance #125821: 2,4-Diamino-6-(hydroxymethyl)pteridine ................ ‘I I 1 1 1 1 I ‘ 1 43 1912 30.80 31.00 31.20 31.40 163 m/z 193.20 12.19% 5000 28 53 68 . 146 175

T’II i 77 92 106 121 133 h . zl, 111 III 4t , , lr | . r , , , ’h | I rll | | ! I m I ! rll | | | I' .L, T I... Tl/Z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 30.80 31,00 31.20 31.40

10209.D SCAN020507.M Tue May 14 14:22:59 2002 Page 6

NYC-WTC_000024342

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NYC-WTC_000024342Source: NYC Law Department, mirrored locally

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