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GCMS analysis results for sample AE10209, May 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10209 conducted on May 20, 2002, including surrogate recovery data.

NYC-WTC_000024333–000024344

Folder label: “GCMS X 5/1/02 A 5/9/02

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NYC 9/11 Public Portal Document

' Data File C:\MSDCHEM\1\DATA\020509\10209.D Vial: 11 Acq On 9 May 2002 8:30 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 2-Chlorocycloheptanone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

24.61 0.51 ug/1 61492 Acenaphthene-dl0 24.46

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Chlorocycloheptanone 146 C7H11C1O 1000194-46-7 27 2 2H-Pyran, 3,4-dihydro- 84 C5H80 000110-87-2 20 3 2H-Pyran, 3,4-dihydro- 84 C5H80 000110-87-2 18 4 2H-Pyranz 3,4-dihydro- 84 C5H80 000110-87-2 18 Abundance Scan 3665 (24.613 min): 10209.0 (-3657) (-) m/ z 55.05 100.00% 55

5000 84 129 43 111 AA Aa a MA A , 1* f 1 1*

n/z-> ................ II l 71 100 -H 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 156 , 180 I " " I " 111''1' I " '11" 24.20 24.40 24.60 24.80 25.00 m/ Z 84.05 49.54% Abundance #14653: 2-Chlorocycloheptanone

Wo 55

41 84 111 5000 T1-r 24.20 24.40 24.60 24.80 25.00 27 68 rn/z 129.10 34.12% 93 102 146

n/z-> , i11" i111 11,1 |l l4 1, IT'1'''1' i l-l-' .'l'l । . .... "131 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 | r " ■ r ‘Ui । < > > 111 <' > ।' > > > । ■ 111

Abundance #111188:2H-Pyran, 3,4-dihydro- 55 ............. ... 27 24.20 24.40 24.60 24.80 25.00 5000 84 m/z 56.10 32.80% 39

69 4444444 '' i' l... . -mmmmmmmmmmmTTTT miz-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 55 #14359: 2H-Pyran, 3,4-dihydro- _A 24.20 24.40 24.60 24.80 25.00 m/z 54.10 32.38% 27 84 5000 39 69

m/z-> 15 TTTTT 4 4 | IIT 111‘511110110917111101011111111113TCB —0"IU33I071 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 24.20 24.40 24.60 24.80 25.00

10209.D SCAN020507.M Tue May 14 14:22:57 2002 Page 5

NYC-WTC_000024341

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NYC-WTC_000024341Source: NYC Law Department, mirrored locally

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