GCMS analysis results for sample AE10208, May 2002

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Laboratory report detailing GCMS analysis of sample AE10208 conducted on May 20, 2002, including surrogate recovery data.

NYC-WTC_000024319–000024332

Folder label: “GCMS X 5/1/02 A 5/9/02”

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\020509\10208.D Vial: 10 Acq On 9 May 2002 7:31 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Morpholine, 4-octadecyl- Concentration Rank 3

y R.T. 38.59 Hit# of EstConc 0.68 ug/1 5 Tentative ID Area 91039 Relative to ISTD Chrysene-dl2 MW MolForm CAS# R.T. 39.94 Qual

1 Moppholine, 4-octadecyl- 339 C22H45N0 016528-77-1 56 2 Diethyl-(1-methyl-3-phenyl-propy... 205 C14H23N 1000194-24-3 40 3 1,3-0xazolidine-2-propanoic .acid... 201 C10H19NO3 1000139-28-1 40 4 4H-Pyran-4-one, tetrahydro- 100 C5H802 029943-42-8 9 Abundance Scan 6044 (38.591 min): 10208.D (-6031) (-) m/z 100.10 100.00% 100

5000

* i ■ • ■ ■ i ■ ■ ■ i ■ 1 38.20 38.40 38.60 38.80 39.00 ..... 43 69 85 1111" 1 r1 ’ ’’113 126 T147 TIT 191 311 —T1110000000000—mmmm—BTT/TET’TT1" m/z 43.10 6.03% mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43779: Morpholine, 4-octadecyl- 100

5000 I ilApuani \ i , AAlA, 38.20 38.40 38.60 38.80 39.00 m/ Z 55.00 6.01%

m/z—> 42743++79 TTT 126141156 184 212 232 252268 294310 338 1 ■ i ■ ■ ■ ■ i " '' r ■ " i'1 " i ■1" i ■ " 11 ‘■ i'''' I' ‘ " i'1' ■ i'' ‘ '"i " 20 40 60 I80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43769: Diethyl-(1 -methyl-3-pheny)-propyl)-amine 100 LAAAAAA— —444A—A4 38.20 38.40 38.60 38.80 39.00 5000 m/z 56.10 5.79%

29 44 72 117134 160 190205 | -HHH —0 0001—— m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43673:1,3-Oxazolidine-2-propanoic acid, 2,3-dimethyl-, e... A 8 MMM A..... 100 38.20 38.40 38.60 38.80 39.00 rn/z 101.20 5.46%

5000 58 156 186 pnigantpunt 841 TIT 28 , . r............... ‘ ।1" ■ m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 38.20 38.40 38.60 38.80 39.00

10208.D SCAN020507.M Tue May 14 14:22:40 2002 Page 8

NYC-WTC_000024330

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