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GCMS analysis results for sample AE10208, May 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10208 conducted on May 20, 2002, including surrogate recovery data.

NYC-WTC_000024319–000024332

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024329
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NYC 9/11 Public Portal Document

"Data File C:\MSDCHEM\1\DATA\020509\10208.D Vial: 10 Acq On 9 May 2002 7:31 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Morpholine, 4-octadecyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 36.51 0.83 ug/1 111622 Chrysene-dl2 39.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Morpholine, 4-octadecyl- 339 C22H45N0 016528-77-1 78 2 Morpholine, 4-[3-(4-butoxyphenox... 293 C17H27NO3 000140-65-8 56 3 Butanamide, 2-(dimethylamino )-N-... 593 C35H39N5O4 018397-13-2 56 4 Isoetharine 239 C13H21NO3 000530-08-5 40 Abundance Scan 5689 (36.505 min): 10208.D (-5679) (-) m/z 100.10 100.00% 100 ft 5000 - 43 36.20 36.40 36.60 36.80 d h ' 1 i ■ 79. 126 168 207 ■ ' i 283........................... m/z 43.10 7.17% n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #43779: Morpholine, 4-octadecyl- KO

5000 AMHABAA, ft । / Yap/wpa,lpi , ) 36.20 36.40 36.60 36.80 m/z 55.10 5.78%

/z-> ..1979. 50 4127156184212 254294 338 ............................................... 1001 150 200 250 300 350 400 450 500 550 600 Abundance #118669: Morpholine, 4-[3-(4-butoxyphenoxy)propyl]- 1(0 128 -44 36.20 36.40 36.60 36.80 5000 m/z 101.20 5.57%

41 70 166 205 236 293 ' ' 111*4 Pr +-r *11" r i” । i i > | < m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #43821: Butanamide, 2-(dimethylamino)-N-[7-(1 H-indol-3-ylm... ' ' I ' ' ' ' I ' 100 36.20 36.40 36.60 36.80 m/ Z 42.10 5.54% 5000

130

/z—> 43.79 50 1 .. J, 170 201229 260 304 3417374 417 451479508 550 593 100 150 200 250 300 350 400 450 500 550 600 36.20 36.40 36.60 36.80

10208.D SCAN020507.M Tue May 14 14:22:38 2002 Page 7

NYC-WTC_000024329

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NYC-WTC_000024329Source: NYC Law Department, mirrored locally

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