GCMS analysis results for sample AE10207, May 2002

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Laboratory report detailing GCMS analysis of sample AE10207 conducted on May 17, 2002, including surrogate recovery data.

NYC-WTC_000024305–000024318

Folder label: “GCMS X 5/1/02 A 5/9/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\020509\10207.D Vial: 9 Acq On 9 May 2002 6:32 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Morpholine, 4-octadecyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 33.84 0.49 ug/1 75770 Phenanthrene-dl0 31.73 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Morpholine, 4-octadecyl- 339 C22H45NO 016528-77-1 64 2 Furaltadone 324 C13H16N4O6 000139-91-3 56 3 1-(2-Morpholinoethoxy)-2-(2-hydr... 295 C16H25NO4 1000215-99-2 40 4 Morpholine, 4-[3-(4-butoxyphenox... 293 C17H27NO3 000140-65-8 40 Abundance Scan 5235 (33.838 min): 10207.D (-5219) (-) m/z 100.20 100.00% 100

5000

43 70 33.60 33.80 34.00 34.20 -#Tp" 126 156 210 256 ‘T1‘‘1‘7111101111111710110‘0917113—30UI‘I3ITCIITI"TT‘3 m/z43.10 8.42% /z—> 20 40 60 80 100 120 140 160 180 200 220.240 260 280 300 320 340 Abundance #43779: Morpholine, 4-octadecyl- KO

5000 y MhpAMaPWr 33.60 33.80 34.00 34.20 m/z 56.10 6.46%

miz-> ,27.43+79 85 126141156 184 212 232 252268 294310 338 " I ■ ’ ’ I 1 " 1 I 1 " ' I 1 1 " I " 1 1 I ITTr I 1 । 1 । I r r । । | i ■ । i | ■ । । । | । i । 'I । । 20 40 60 80 100 12Q 140 160 180 200 220 240 260 280 300 320 340 Abundance #118637: Furaltadone 1(0 1 33.60 33.80 34.00 34.20 5000 m/z 101.10 5.97%

—416, 79 Ip-n i |1 1 1T i Ci ■ i ■ > 128 185 ■ ■। ■11111" ■ I'1" ir... .. ................ .. .. .. ■ i■' " i ■ ■ ■ ■ i ■■'■i1■■■ i■ ■ ■11 ■ ■ m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43636:1 -(2-Morpholinoethoxy)-2-(2-hydroxy-1 -phenylethoxy... A A,, • 1 I ’ ’ 100 33.60 33.80 34.00 34.20 m/z 41.10 5.12% 5000

nfe-> 20 56 77 ----- “, "120 144 176193 264 11 ‘ " i1' " i " '11 “ " I " '111'" I " " I ITTi 11" 1 IT 1 ■ 11 > ।' j 11 40 60 80 100 120 140 160 180 200 220 240 260280 300 320 340 AllahutuMulndua 33.60 33.80 34.00 34.20

10207 .D SCAN020507.M Tue May 14 14:22:16 2002 Page 6

NYC-WTC_000024314

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