GCMS analysis results for unknown compounds, sample AE10202, May 2002

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Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10202 on May 10, 2002.

NYC-WTC_000045020–000045044

Folder label: “GCMS X 4/30/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10202.D Vial: 20 Acq On 9 May 2002 6:53 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 10 Morpholine, 4-octadecyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

24.24 0.62 ug/L 1067290 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Morpholine, 4-octadecyl- 339 C22H45NO 016528-77-1 72 2 Butanamide, 2-(dimethylamino)-N-... 593 C35H39N5O4 018397-13-2 4 3 Furaltadone 324 C13H16N406 000139-91-3 / 9 4 1-Propanone, 2-(diethylamino)-1-.. . 205 C13H19NO 000090-84-6 39 Abundance Scan 3601 (24.237 min): 10202.D (-3593) (-) m/z 100.10 100.00% 100

5000

• ‘ I ’ • l 1 1 1 ' i r ' 24.00 24.20 24.40 24.60 0- 41.70, . '-B————m——T—m——OTm—WWWITTT i r ['*i T ~i r~f t 126 210 255 m/z 101.10 5.19%' m/z-> 50 100i 150 200 250 300 350 400 450 500 550 600 Abundance #43779: Morpholine, 4-octadecyl- 100

5000 1 1 ■ ' ■ i 1 1 24.00 24.20 24.40 24.60 m/z 41.10 4.89% 0 .4370), 127156184212 254 294 338 । । । । । i i > । i ■ । । | > । । । । । । 1 l । i i । i i । i । । i n । i i i C i । i i— । । m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #43821: Butanamide, 2-(dimethylamino)-N-[7-(1H-indol-3-ylm... 100 1MMAMMkAMA"Mn 11111 r i | I i I i | i i i i । i i I

24.00 24.20 24.40 24.60 5000 m/z 43.10 4.02%

m/z-> Abundance 01 42 ■70 1 "1“ 50 । । * t 130 170 201229 260 304 347374 417 451479508 550 593 — r-t-r1 I I 11 I [ I 1 I I 1“I I I I I I I I I I I I I I ] I I I I I I I I I I T 100 150 200 250 300 350 400 450 500 550 600

100 #118637: Furaltadone AL m/ z 24.00 24.20 24.40 24.60 56.10 3.58% 5000

56 128 185 0 ■ ■ i ■ ■ ■■ ■ i ■ ■ ■ ■ t ■ ■ ■ ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ > । . I । ' ■ । । । ............ ,4. m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 24.00 24.20 24.40 24.60

10202.D 050102.M Thu May 09 13:37:32 2002 Page 14

NYC-WTC_000045040

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NYC-WTC_000045040Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AE09971, May 2002 · Box DEP Box 25

NYC-WTC_000044071

Laboratory report for sample AE09971 showing surrogate recovery and unknown compounds from May 9, 2002.

1 shared topics · Same agency, volume and box · similarity 0.996