GCMS analysis results for unknown compounds, sample AE10202, May 2002

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Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10202 on May 10, 2002.

NYC-WTC_000045020–000045044

Folder label: “GCMS X 4/30/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\10202 . D Vial: 20 Acq On 9 May 2002 6:53 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Morpholine, 4-octadecyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 29.09 0.37 ug/L 543985 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Morpholine, 4-octadecyl- 339 C22H45NO 016528-77-1 78 2 Furaltadone 324 C13H16N4O6 000139-91-3 43 3 Imidazole, 5-fluoro-4-methyl- 100 C4H5FN2 041367-01-5 9 4 6-Undecylamine 171 C11H25N 033788-00/0 9 Abundance Scan 4427 (29.090 min): 10202.D (-4406) (-) m/z 100.10 100.00% 100

5000

1 1 I ' ' 1 1 I ' 1 43 28.80 29.00 29.20 29.40 l„ 69 84 7 i 7 j i I i i-1 l rr 1' । r V r i 11 i m । ft । । | i n । | । । r । । i r । t । i । । । i i । । । । । । < । | rr m/ z 43.05 6.52% r 1111 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43779: Morpholine, 4-octadecyl- 100

MMMAMpPrw WhMMm 5000 1 1 ' I 1111 1 1 1 ' 1 I ' ' ' I I ' ' 1 28.80 29.00 29.20 29.40 m/z 55.10 5.39% 27 43 70 85 0- | i i I | [ I I i T [ i it i | li i i 126141156 184 212 232 252268 294310 । । । । । । । । । । । I । । । । । । । । । । । । < i । prri i । Fes > । । । । । । i । r i । i । । i । i i i । 338 i i

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #118637: Furaltadone 100

5000 m/z 101.10 5.32%|

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43772: Imidazole, 5-fluoro-4-methyl- 7 । | i । । y । i i f [ i i i i J' i r 100 28.80 29.00 29.20 29.40 m/ z 41.10 4.23%| 5000 42 72 I 57 J, 0 | । i । |I T I | I i | ITII i । i i-1 | n i । । । । । । [ । i । < । i । । f । । i । । | । 1 । [ । i i । | । । i । । i । । । । । i r i । । । । । । । r

miz- 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 28.80 29.00 29.20 29.40

10202.D 050102.M Thu May 09 13:37:39 2002 Page 18

NYC-WTC_000045039

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NYC-WTC_000045039Source: NYC Law Department, mirrored locally

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