GCMS analysis results for sample AE11930, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11930.D Vial: 10 Acq On : 23 May 2002 5:18 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Imidazol, 4-fluoro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 3.75 3.25 ug/L 1908710 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua.

1 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0 A 2 Ethyl Chloride 64 C2H5C1 000075-00-3/4 3 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-/ 2 4 1,4-Pentanediamine, N1,N1-diethyl- 158 C9H22N2 000140-80/7 2 Abundance Scan 114 (3.749 min): 11930.D (-111) (-) m/z 49.10 100.00% 49

86 5000 40 ' 1 i ■ ■ 1 1 i ‘ ■ i 1 1 1 1 i 1 1 1 1 I 1 58 3.40 3.60 3.80 4.00 0: r'' f • • I I | 1 1 1 > 1 > * < • | > ' - 4 m/z 48.10 55.23% n/z->10 Abundance 20 30 40 50 60 70 #34862: Imidazol, 4-fluoro- 80

86 90 100 110 120

manu/"MoMM.ko 5000 T ■’“T' 3.40 3.60 3.80 4.00 59 m/z 86.00 51.02%

Ot 10 pi । । i । । i । । । i । ■ i ■ ■ ■ ‘ i ■ ■ • ■ i ■ ‘ ' ■ i ■ ■

rnfz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #107943: Ethyl Chloride 23 ‘ ‘ i • ■ • • I ‘ ■ I ' • 1 ■ i ■ • ■ ■ i ■ 3.40 3.60 3.80 4.00 64 5000 m/z 40.10 34.88? 49 35

miz-> 15 Of ■ ■ ■ l all, 111 10 20 30 I + 40 50 60 70 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■' ।

80 90 100 ‘ ‘ i ■ ■ ■ ■ i • ■

110 120 Abundance #1082: Ethanol, 2,2-dichloro- 31 3.40 3.60 3.80 4.00 1 m/ z 84 ..00 30.23% 5000

25 . 37 43 4% 55 61 70 77 83 96 103 114 0 TIITT TT m/z—> 10 20 30I 40 50 60 70 80 90 100 110 120 3.40 3.60 3.80 4.00

11930.D 052202.M Wed May 29 09:50:18 2002 Page 6

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