GCMS quantitation report, sample LB, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\061102\LB.D . Vial: 4 Acq On : 11 Jun 2002 12:19 pm Operator: Sample : gc/ms scan 6/11 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Imidazol, 4-fluoro- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 3.99 1.36 ug/L 1014270 1,4-dichlorobenzene-d4 9.89

Hit# of Tentative ID MW MolForm CAS# Qual 1 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0 2 2 1,4-Pentanediamine, N1 ,N1 -diethyl - 158 C9H22N2 000140-80-7 1 3 Amprotropine 307 C18H29NO3 000148-32-3 1 4 Diethazine 298 C18H22N2S 000060-91-3 1 Abundance / Scan 155 (3.990 min): LB.D (-153) (-) m/z 49.10 100.00% 49 86

5000

40 56 3.60 3.80 4.00 4.20 4.40 0-1 ■ l it] ■' ll| ■ -7PP I m/z 86.00 72.28% niz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #34862: Imidazol, 4-fluoro- 86

5000 3.60 3.80 4.00 4.20 4.40 59 m/z 56.10 7.54% 0-—OPTPPIPTT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #116808:1,4-Pentanediamine, N1,N1-diethyl- 86 ■ i 1 ■ ■ ■ i ■ ■ • * i ■ i ■ 3.60 3.80 4.00 4.20 4.40 5000- m/z 50.00 6.65%

mfz~> 0- 11' i'11 11 30 40 58 45 , 65,42.. . 1111198'T1111112 50 60 70 129 143 158 1 L > ■ i11II 111111 11111 ''i11 80 90 100 110 120 130 140 150 160 w"My"nyas Abundance #34953: Amprotropine 86 3.60 3.80 4.00 4.20 4.40 m/z 86.95 5.52% 5000

58 72 0- ■' i ■ ‘ '11 ■ ■ • ■ i ■ • H i11111111111' 1 103 121 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 3.60 3.80 4.00 4.20 4.40

LB.D 060302.M Tue Jun 11 15:54:56 2002 Page 8

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