GCMS analysis results, sample AE09771, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \MSDCHEM\1\DATA\050602\9771.D Vial: 24 Acq On 7 May 2002 6:25 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Imidazol, 4-fluoro­ Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.92 0.41 ug/L 242507 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0 2 2 2- [4-Chloro-2-nitrophenyl] -1-die.. . 399 C21H22C1N3O3 1000212- 69-9 1 3 Nitrosyl chloride 65 CINO 002696 2-6 1 4 Butanedial 86 C4H602 000638 -37-9 1 Abundance Scan 143 (3.920 min): 9771 .D (-136) (-) m/ z 35.1/0 100.00% 35

AN 86 5000

"IT "II 58 3.60 3.80 4.00 4.20 ILL ' F1 " 111 1’0"m00’"0011110111111011111111111111111112111111110111111111173211111121277117T m/z 86.00 50.26% m/z-> Abundance 20 40 60 80 100120140160180200220240260280300320340360 380400 #34862: Imidazol, 4-fluoro- /MMMMrMyA 85 ww-

5000 1 1 1 1 1 1 1 ' I 1 1 1 1 I 1 1 11 I ■ ' 1 1 I 3.60 3.80 4.00 4.20 m/z 40.10 49.57% 59

m/z-> 20 40 60 80 100120140160180200220240260280300320340360 380400 Abundance #34812: 2-[4-Chloro-2-nitrophenyl]-1 -diethylaminoethyl-3-f... 86 -‘ 1 ■ i ■ ' ■ ■ i 1 1 ■ ' i 1 ‘ ■ 1 i ' 1 1 ■ । 3.60 3.80 4.00 4.20 5000 m/z 84.95 14.11%

117138 ' i1' " 11" j 176 203 238 266 313 111"1 r 1111111 Tp-rTTp-rTTp-rTTp-TTTp-rTTp-rT-rp-rTTp-r^^ 399 A A mfe-> 20 40 60 80 100120140160180200220240260280300320340360380400 Abundance #713: Nitrosyl chloride 33 3.60 3.80 4.00 4.20 m/z 37.10 11.70%

5000 Al

49 T i■ i" • ■ i11 ■111"11 I" " T i111' i"11111" r 1111 I''1' I'11 ■' p1'' I r "11 I’ TT m/z-> 20 40 60 80 100120140160180200220240260280300320340360380400 3.60 3.80 4.00 4.20

9771.D 050102.M Tue May 07 15:44:21 2002 Page 8

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