GCMS analysis results for sample AE12092, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052302\12092.D Vial: 13 Acq On : 23 May 2002 7:45 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Imidazol, 4-fluoro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.95 2.75 ug/L 1728380 1,4-Dichlorobenzene-d4 9.90

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0 4 2 Borane, trifluoro- 68 BF3 007637-07-2 2 3 Ethyl Chloride 64 C2H5C1 000075-00-3 2 4 Boron trifluoride etherate 142 C4H10BF3O 000109-63-7 2 Abundance Scan 148 (3.949 min): 12092.D (-146) (-) m/z ,49.10 100.00% 43

86 5000 82 44 ■ ■ i ■ • ■ ■ i ■ ■ ■ ■ i ' ■ ■ ■ i ■ ■ ■ ' i 1 3.60 3.80 4.00 4.20 0-■ i .,।■ j. 3740 I ।।....!.... r,... [. 1 >< ।. TmTTTTTTTTTT + ) m/z 86.00 61.50% miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #34862: Imidazol, 4-fluoro- 85

5000 ■ ■ i ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ ' 1 i ■ ■ ■ ■ i • 3.60 3.80 4.00 4.20 59 m/z .84.00 59.67%

OhmmPDm]0PmmmmTpp —p] mfe-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12321: Borane, trifluoro- 49 ' ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । • ■ ■' । ■ ■ ■ ■ ।1 3.60 3.80 4.00 4.20 5000 m/z 47.10 52.67%

11 19 30 38 68 Oh TT—mmmmnn—m—mmB—Bu7T ThmmITRRTITTTTTT miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #107943: Ethyl Chloride ' ■ i ■ ■ ■ ■ i ■ • ■ ■ i ■ ■ 1 ■ i • ■ ■ ‘ i ‘

3.60 3,80 4.00 4.20 m/z 81.90 36.50% 64 5000

49

n/z—> 1215 25 35 7 Of-44 TH 31..438,-4741.., 1’1001-1011121110111103092337717 o 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ulMAhab Mukk—lll 3.60 3.80 4.00 4.20

12092.D 052202.M Wed May 29 09:52:18 2002 Page 8

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