GCMS calibration table data, sample AE10517, May 22, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Imidazol, 4-fluoro- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 3.86 1.34 ug/L 837793 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0/4 2 3-Aminopropionitrile 70 C3H6N2 000151-18 ' 3 3 Propiolonitrile 51 C3HN 001070-71 4 Pent-3-enylamine 85 C5H11N 087156-70 Abundance Scan 133 (3.861 min): 10517.D (-131) (-) 85 m/z 86.00 10 2, 49

5000 36 42 70 58 3.60 3.80 4.00 4.20 Of . 4 li11.1 — HmIT m/z 49.10 77.90% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #34862: Imidazol, 4-fluoro- 85

5000 3.60 3.80 4.00 4.20 59 m/z 51.10 77.72% 01 "i “ •' i ■ ■ ‘' l1 “ ‘ i “ "i “ ‘' i‘" ‘ i ‘' i' ”' i'' ■ ‘i ■ ■ “ i“ । *i‘ i ‘"i “ “i ■' ■' i■ ■' ■ i —pp Tl/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #680:3-Aminopropionitrile 33

3.60 3.80 4.00 4.20 5000 m/z 84.90 68.54%

■nfe-> 04

Abundance 42 121518 2427 3336391 45 52 TITTuphe 1 ■111 “ 1111 6669 1' • i “ ■ • i11" I ‘"1111111'1 ’ 'Trn >'1' “ 11 “ 111111 > 111111 > 5 10 15 20253035 40 4550556065 70 75 80859095 #12371: Propiolonitrile WA+hAws, 51 3.60 3.80 4.00 4.20 m/z 42.05 36.70% 5000 MW 0- -rrp-r .................................................... N—unmOmmmaumm /z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

10517.D 052202.M Wed May 22 11:48:05 2002 Page 5

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