GCMS analysis results for sample AE11932, June 2002

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Laboratory report documenting GCMS analysis of sample AE11932 conducted on June 5, 2002.

NYC-WTC_000013666–000013694

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\DATA\052302\11932.D Vial: 12 Acq On : 23 May 2002 6:56 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 18 4,9-Decadien-2-amine, N-butyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

24.20 0.96 ug/L 998844 Phenanthranene- dl 0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

14,9-Decadien-2-amine, N-butyl- 209 C14H27N 062238-25-9 72 (2 Morpholine, 4-octadecyl- 339 C22H45NO 016528-77-1/64 3-Fural t adone 324 C13H16N4O6 000139-91-3 50 4 1-(2-Morpholinoethoxy) -2-(2-hydr... 295 C16H25NO4 1000215-99-2 39 Abundance Scan 3595 (24.202 min): 11932.D (-3587) (-) m/z 100.10 00.00% 100

5000

23.80 24.00 24.20 24.40 24.60 41.56..84, 0+ I’*’ ’11 ’’114 ’ ’10* 1 126 255 210 1’1111111111111111111101071/61731 " i ■ “ ■ i‘ • i “ 1 ‘‘i “ ■ • i m/z 101.10 5.98% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43598: 4,9-Decadien-2-amine, N-butyl- 100

5000 44 23.80 24.00 24.20 24.40 24.60 m/z 41.20 4.83%

niz—> 0 4.459,81.. 123138 166 194210 ■' i" “ i ■ •" i ‘11" " i “ ■ • i " ■ ■ i “ " 111" i ‘ “ 1111111 “ “ I " 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43779: Morpholine, 4-octadecyl- KO . /y.. 23.80 24.00 24.20 24.40 24.60 5000 m/z 43.10 4.46%

/z-> 0 27.43+79.85 126141156 184 212 232 252268 294310 338 ’’I’*’’I’42*1**’*1*4**I’**’I—IIIIII7/7 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance KO #118637: Furaltadone AA— 44 23.80 24.00 24.20 24.40 24.60 m/z 55.10 3.35% 5000

0 41 56 . 79 -pmmm 111 128 185 TTT ' ' | ‘ ' I r" ' I “ ‘ ‘ I ' " ‘ I ‘ ‘ I ' 1 “ I ‘ ‘ I ' “ ‘ ‘ ' t “ i ‘ ■ i ■ ■ i ■ ■ • ‘ i ■ ■ iz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 23.80 24.00 24.20 24.40 24.60

11932.D 052202.M Wed May 29 09:51:38 2002 Page 21

NYC-WTC_000013692

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NYC-WTC_000013692Source: NYC Law Department, mirrored locally

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NYC-WTC_000013454

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