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GCMS analysis results for sample AE11932, June 2002

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Laboratory report documenting GCMS analysis of sample AE11932 conducted on June 5, 2002.

NYC-WTC_000013666–000013694

Folder label: “GCMS X 5/22/02 A 5/23/02

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NYC 9/11 Public Portal Document Tentatively Identified Compound (LSC) summary . * Operator ID: Mclean Date Acquired: 23 May 2002 6:56 pm Data File: C:\MSDCHEM\l\DATA\052302\11932.D Name: 5/22ad Mise: Method: C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone Methylene Chloride 3.72 2.3 ug/L 1585340 1 9.90 27384800 40.0 1,3-Dioxol-2-one 3.75 0.7 ug/L 466955 1 9.90 27384800 40.0 Methane, chloro­ 3.77 0.7 ug/L 487108 1 9.90 27384800. 40.0 Methylene Chloride 3.79 1.1 ug/L 765638 1 9.90 27384800 40.0 2-Imidazolidinone 3.83 0.7 ug/L 446472 1 9.90 27384800 40.0 Acetic acid, chlo... 3.85 0.8 ug/L 518187 1 9.90 27384800 40.0 4H-1,2,4-Triazol-... 3.88 1.8 ug/L 1225150 1 9.90 27384800 40.0 Toluene 4.27 1.2 ug/L 818365 1 9.90 27384800 40.0 Methylene Chloride 4.43 0.5 ug/L 367165 1 9.90 27384800 40.0 Pyridine-d5- 4.48 0.5 ug/L 338402 1 9.90 27384800 40.0 Methylene Chloride 4.52 0.5 ug/L 329956 1 9.90 27384800 40.0 4H-1,2,4-Triazol-. . . 4.79 0.3 ug/L 215422 1 9.90 27384800 40.0 4-Methyl-5-nitro-... 5.02 0.3 ug/L 195483 1 9.90 27384800 40.0 Cyclotrisiloxane, ... 5.36 0.4 ug/L 241488 1 9.90 27384800 40.0 2-Pentanone, 4-hy... 5.93 10.0 ug/L 6880160 1 9.90 27384800 40.0 Phenanthrene, 9-m... 22.54 0.3 ug/L 281690 4 22.91 41564500 40.0 Phenanthrene-dl0 23.07 0.2 ug/L 245226 4 22.91 41564500 40.0 4,9-Decadien-2-am... 24.20 1.0 ug/L 998844 4 22.91 41564500 40.0

11932.D 052202.M Wed May 29 09:51:38 2002 Page 22

NYC-WTC_000013693

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NYC-WTC_000013693Source: NYC Law Department, mirrored locally

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