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GCMS quantitation results for sample AE10241, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE10241 conducted on May 28, 2002.

NYC-WTC_000024780–000024790

Folder label: “GCMS X 5/14/02 A 5/17/02

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Scanned page image, NYC-WTC_000024788
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10241.D Vial: 19 Acq On : 10 May 2002 4:25 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Morpholine, 4-[3-(4-butoxyp... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 36.51 1.02 ug/1 111128 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Morpholine, 4-[3-(4-butoxyphenox... 293 C17H27NO3 000140-65-8 72 2 Furaltadone 324 C13H16N4O6 000139-91-3 72 3 Morpholine, 4-octadecyl- 339 C22H45NO 016528-77-1 72 4 .alpha.-Hydroxybenzenebutanamide... 292 C16H24N2O3 1000194-56-6 56 Abundance Scan 5689 (36.505 min): 10241 .D (-5681) (-) m/z 100.10 100.00% 100

5000

43 36.20 36.40 36.60 36.80

/z—> H79485— 20 40 60 126 170 1' r '1 ■ i ■ " ‘ I ' r ' " i " '' i 282 ■ i ■' " i'11' i1' " i1 " ■ i11111" m/z 43.10 6.49% 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #118669: Morpholine, 4-[3-(4-butoxyphenoxy)propyl]- 100 128 winllkqtnqqH Wyhanuooo 5000 36.20 36.40 36.60 36.80 m/z 41.10 6.35% 41 70 TTTTI111, 185 , n 150166 205 236 293 I'11111 11111 TT * ■ i1' ■ • 1 ■ ■ ■ ■ । ■i•■ • ■। " i • • ’' i " " i " ■11 • • ’ ■ i ■ ■ " i' ■ m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #118637: Furaltadone 100 Nada 4 hh 1 Mil "YmAnaA Ak 36.20 36.40 36.60 36.80 5000 m/z 101.20 5.40%

m/z—> —49. 79 ■ i ■ ■ 128 185 TTTUTTTTTTTTTTTTLIITTTITTTTT 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 - Abundance #43779: Morpholine, 4-octadecyl- 100 36.20 36.40 36.60 36.80 m/z 56.00 5.39% 5000

m/z-> 27,.43+.79./85 126141156 184 212 232 252268 294310 338 1 ‘ i ‘ ‘' i'''' i " '' i ‘ " 11 “ '' i ■ ‘1' i' ■ " i ‘1111" 11111111111 '"11' 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 AAAA ' "414 ′ ' * i ’ A A 'i 1 1 ■ 'i 36.20 36.40 36.60 36.80

10241.D SCAN020507.M Tue May 14 14:25:39 2002 Page 7

NYC-WTC_000024788

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NYC-WTC_000024788Source: NYC Law Department, mirrored locally

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